2021
DOI: 10.1016/j.foodchem.2020.128650
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Zirconium(Ⅳ)-based metal-organic framework for determination of imidacloprid and thiamethoxam pesticides from fruits by UPLC-MS/MS

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Cited by 42 publications
(8 citation statements)
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“…Gas 1 and Gas 2 were both 55 Psi, the IS was 4500 V, the ionization temperature was 600°C, the curtain gas was 25 Psi, the collision voltage was 25 V, and the chamber injection voltage was 15 V. Data analysis was performed using AnalystTM1.6 software and MultiQuantTM3.0 software (American AB SCIEX). Eventually, the compounds with |ΔPPM | < 15.0 were derived ( Xu et al, 2021 ).…”
Section: Methodsmentioning
confidence: 99%
“…Gas 1 and Gas 2 were both 55 Psi, the IS was 4500 V, the ionization temperature was 600°C, the curtain gas was 25 Psi, the collision voltage was 25 V, and the chamber injection voltage was 15 V. Data analysis was performed using AnalystTM1.6 software and MultiQuantTM3.0 software (American AB SCIEX). Eventually, the compounds with |ΔPPM | < 15.0 were derived ( Xu et al, 2021 ).…”
Section: Methodsmentioning
confidence: 99%
“…This result was basically consistent with the literature data. 42 The XRD patterns of Fe 3 O 4 and Fe 3 O 4 @UiO-66-NH 2 are shown in Fig. 2(d).…”
Section: Methods Validationmentioning
confidence: 99%
“…Due to the high surface area, large pore volume, and excellent stability in the water and acid conditions, UiO-66 ( Cao et al, 2018 ) was used as the dSPE sorbent to extract IMI, ACE, THI, THX, CLO in water samples. Moreover, the addition of amino groups on UiO-66 (UiO-66-NH 2 ( Xu et al, 2020 )) may increase the electrostatic interactions between the sorbent and analytes, allowing efficient extraction of IMI and THX from fruit samples. The amount of adsorbent (≤50 mg) used for dSPE is significantly less than that of the SPE column, and the dSPE also has a satisfactory recovery.…”
Section: Sample Pretreatmentmentioning
confidence: 99%
“… Analyte Sample Extractant SPE Salt pH Reuse Elution Detection Recovery Ref. IMI, ACE, THI, THX, CLO Water / UiO-66 (40 mg) 15% NaCl 9 10 3 mL acetone LC-MS/MS 73.7–119.0 Cao et al, (2018) IMI, ACE, THI, THX, CLO Fruit juice, water / Montmorillonite (30 mg) 0.03 g Na 2 SO 4 4 4 0.15 mL 70% ACN HPLC-DAD Khwankaew et al 2018 IMI, THX Fruit ACN UiO-66-NH 2 (50 mg) / 9, 5 8 3 mL ACN (0.1% methanoic acid) UPLC-MS/MS 86–107 Xu et al, (2020) IMI, ACE, THI, THX Lemon juice / Magnetic 3D-graphene (15 mg) / 7 20 0.3 mL acetone LC-UV 88.75–111.60 Liu et al, (2014) IMI, ACE, THI, THX, CLO, DIN Water / Fe 3 O 4 /GO/ZIF-67 (40 mg) / 7 1 mL ACN LC-MS/MS 83.5–117.0 Cao et al, (2017) IMI, ACE, THI, CLO Water / Magnetic porous porphyrin organic polymer (15 mg) 7 5 1.13 mL ACN LC-DAD 91–99.3 Selahle et al, (2020) IMI, ACE, THI, ...…”
Section: Sample Pretreatmentmentioning
confidence: 99%