Organic Syntheses 2003
DOI: 10.1002/0471264180.os029.06
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α‐Bromoheptaldehyde

Abstract: α‐Bromoheptaldehyde reactant: 285 g. (335 ml., 2.5 moles) of heptaldehyde intermediate: heptaldehyde enol acetate intermediate: α‐bromoheptaldehyde dimethyl acetal product: α‐bromoheptaldehyde

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(7 citation statements)
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“…Flash chromatography (cyclohexane/ethyl acetate gradient from 99:1 to 90:10) followed by bulb-to-bulb distillation gave 7.88 g of pure compound 33 (58%). 1…”
Section: (±)-Hexyl 2-oxocyclohexanecarboxylate (28)mentioning
confidence: 99%
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“…Flash chromatography (cyclohexane/ethyl acetate gradient from 99:1 to 90:10) followed by bulb-to-bulb distillation gave 7.88 g of pure compound 33 (58%). 1…”
Section: (±)-Hexyl 2-oxocyclohexanecarboxylate (28)mentioning
confidence: 99%
“…Obtained in 25% yield according to the general procedure above. 1 (t, J = 7.6, 2 H). ; 13 C NMR, (enol form) 14.0 (q); 21.7 (t); 22.6 (t); 22.9 (t); 23.9 (t); 24.0 (t); 31.2 (t); 31.6 (t); 36.9 (t); 106.…”
Section: (±)-2-hexanoylcyclohexanone (35)mentioning
confidence: 99%
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