Селективный синтез γ-WO
 
 3
 
 и β-WO
 
 3
 
 ⋅ H
 
 2
 
 O гидротермальной обработкой пероксовольфрамовой кислоты

Бушкова, Т. М.; Egorova, A. A.; Хорошилов, А.; Иванова, О. С.; Япрынцев, А. Д.; Баранчиков, А. Е.; Иванов, В. К.

doi:10.31857/s0044457x21040073

Ж. неорган. химии

2021

DOI: 10.31857/s0044457x21040073

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Селективный синтез γ-WO ₃ и β-WO ₃ ⋅ H ₂ O гидротермальной обработкой пероксовольфрамовой кислоты

Т. М. Бушкова¹,

A. A. Egorova²,

А. Хорошилов³

et al.

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Hydrothermal Synthesis and Photocatalytic Properties of Cobalt-Doped Tungsten Oxide

Zakharova,

Podval’naya,

Gorbunova

et al. 2023

Žurnal neorganičeskoj himii

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Hexagonal tungsten trioxide–base interstitial solid solutions of general formula CoxWO3, where 0.01 ≤ x ≤ 0.09, were prepared hydrothermally. The dopant homogeneity extent was found to depend on рН in the working solution. Interstitial solid solutions with the highest Co2+ concentrations were formed at рН of 2.3. The CoxWO3 samples with a fiber-like morphology with a fiber diameter of ca. 40 nm, which were prepared at рН of 2.3, had the highest specific surface area, equal to 38.6 m2/g. The key parameter for the stability of the CoxWO3 crystal structure appeared to be ammonium ions residing in the hexagonal channels of the crystal structure. When tested as photocatalysts of 1,2,4-trichlorobenzene oxidation under the UV light, the prepared samples showed high chloroarene conversions and low selectivities to yield a wide range of organic compounds, including chlorine-free ones.

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Hydrothermal Synthesis and Photocatalytic Properties of Cobalt-Doped Tungsten Oxide

Zakharova,

Podval’naya,

Gorbunova

et al. 2023

Žurnal neorganičeskoj himii

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show abstract

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Селективный синтез γ-WO ₃ и β-WO ₃ ⋅ H ₂ O гидротермальной обработкой пероксовольфрамовой кислоты

Cited by 1 publication

References 0 publications

Hydrothermal Synthesis and Photocatalytic Properties of Cobalt-Doped Tungsten Oxide

Hydrothermal Synthesis and Photocatalytic Properties of Cobalt-Doped Tungsten Oxide

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Селективный синтез γ-WO 3 и β-WO 3 ⋅ H 2 O гидротермальной обработкой пероксовольфрамовой кислоты

Cited by 1 publication

References 0 publications

Hydrothermal Synthesis and Photocatalytic Properties of Cobalt-Doped Tungsten Oxide

Hydrothermal Synthesis and Photocatalytic Properties of Cobalt-Doped Tungsten Oxide

Contact Info

Product

Resources

About

Селективный синтез γ-WO ₃ и β-WO ₃ ⋅ H ₂ O гидротермальной обработкой пероксовольфрамовой кислоты