In this research, nanocellulose is isolated from Moringa oleifera seed using acid hydrolysis and the structural properties were determined. X-ray diffraction (XRD) and Fourier transform infrared (FTIR) spectroscopy were used for the characterization of the isolated nanocellulose. The most noticeable peak is observed at and the value of the crystallinity index () from the XRD pattern is 63.1%. The calculated values of hydrogen bond intensity (HBI), lateral order index (LOI) and total crystalline index (TCI) are 0.93, 1.17and 0.94 respectively exhibited high degree of crystallinity and well arranged cellulose crystal structure. The isolated nanocellulose has an average length and diameter of 14.3 and 36.33 respectively. Furthermore, the FTIR peaks revealed the presence of C-H bending, C-O stretching and O-H stretching functional groups.
The use of Moringa oleifera seeds for purifying water has been attempted locally in various forms without putting scientific potency of the material into consideration. The cellulose sample isolated from Moringa {oleifera} seed was characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transform infrared spectroscopy (FTIR). The value of the crystallinity index (CIr ) from the XRD pattern is 63.1%. The high degree of crystallinity obtained is attributed to the high percentage of crystallinity index, CIr (i.e. 63.1%). The morphology revealed aggregates of conical and needle-like structure. The FTIR revealed O-H stretching, C-H stretching vibration, and C=O bond stretching functional groups. These characteristics are indicative of the potential of the material in water purification.
In this work, the Specific Energy Consumption (SEC) and machine capacity for a Moringa oleifera seed shelling machine were determined in relation to the cylinder speed and seed sizes. A M. oleifera seed shelling machine was tested and the SEC was appraised. The SEC and machine capacity of the M. oleifera seed shelling machine were determined at five speed levels, viz. 200, 240, 280, 320 and 360 rpm using three seed sizes (viz. small, medium and large seed sizes). The SEC and machine capacity increased with the seed sizes during the shelling process. The same trend was observed for the relationship between the SEC and cylinder speed. The minimum values obtained for the SEC using the small, medium and large M. oleifera seed sizes were 31.25, 40.07 and 54.22 Wh·kg<sup>–1</sup>, respectively, at a cylinder speed of 200 rpm while the maximum values obtained for the small, medium and large seed sizes were 58.01, 74.37 and 100.63 Wh·kg<sup>–1</sup>, respectively, at a cylinder speed of 360 rpm. The optimum values obtained for the machine capacity were 14.58, 11.38 and 8.41 kg×h<sup>–1</sup> using the small, medium and large seed sizes, respectively. Conclusively, this study shows that the SEC and machine capacity were affected by the variation in the cylinder speed and seed sizes.
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