The aim of the present work was to determine the influence of the retrogression and reaging (RRA) heat treatment on the correlation between microstructure, mechanical properties and susceptibility to stress corrosion cracking (SCC) of the AlZn5Mg1 alloy in dry air and sea water. The alloy received in the T6 temper was subjected to 9 different heat treatments, including retrogression at temperature 453 -513 K for 600 -3600 s, and reaging at temperature 363 K or 403 K for 16 h, 24 h or 48 h. The susceptibility to SCC was investigated by slow strain rate tensile tests at 10 À6 s À1 strain rate; change in time to failure, fracture energy and reduction in area were taken into account. Generally, the heat treatment improving mechanical properties increased susceptibility to SCC. The observed effects were discussed in terms of change in microstructure, especially size and distribution of phase precipitates. The role of change in dislocation network was the most likely of no importance.
In the present work the evolution of the morphology (examined by means of SEM ) and changes in the chemical composition (examined by means of EDS microanalysis) of the intermetallic phases precipitates, containing Fe and Mn, in AA3004 type alloy, slowly cooled and frozen at 580, 510 and 430 °C, was analysed. The morphology of the intermetallic phase particles, depending on their chemical composition and precipitation temperature, was determined. It has been stated that intermetallic phases Al 6FeMn and a-Al(FeMn)Si, of different stoichiometry, precipitate at successive stages of solidification and cooling. The a-Al(FeMn)Si phase particles chinese script (Fe/Mn=2.3, [Fe+Mn]/Si=2.1-2.5) and branches (Fe/Mn=2.7-3.1, [Fe+Mn]/Si=2.3) were observed.
The aim of the study was to design and optimize the complex, two-step heat treatment of Cu-Ni (Mn, Mo) ductile iron. A method for the formation and investigation of austempered ductile iron (ADI) by means of complex two-step and as comparative, standard one-step heat treatments has been developed, using quenching dilatometer. Investigations of proceeding phase transformations using differential dilatometric and DSC analysis supported by microstructural observations, hardness and austenite volume measurements have been carried out. An analysis of the temperature sequence of the ausferrite decomposition in the one-step and two-step ADI was performed, which allowed for the separation and identification of the effects responsible for the carbon-enriched austenite decomposition. A quantitative relationship was established between basic dimensional effects revealed on the differential dilatometric curve of ausferrite decomposition, which enables prognosis and optimization of the parameters of complex ADI heat treatment variants. Verification tests were performed on a stand equipped with salt furnaces enabling a quick transfer of samples from one bath to another without changing their initial temperature. Optimization of the two-step ADI heat treatment with the use of quantitative dilatometric analysis of the ausferrite decomposition, allowed to obtain for the temperature step-down heat treatment 390°C/15, 20 min ) 270°C/130 min the excellent mechanical properties, unattainable by means of standard 1-step ADI heat treatment.
Combination of extreme service conditions and complex thermomechanical loadings, e.g., in electronics or power industry, requires using advanced materials with unique properties. Dissipation of heat generated during the operation of high-power electronic elements is crucial from the point of view of their efficiency. Good cooling conditions can be guaranteed, for instance, with materials of very high thermal conductivity and low thermal expansion coefficient, and by designing the heat dissipation system in an accurate manner. Conventional materials such as silver, copper, or their alloys, often fail to meet such severe requirements. This paper discusses the results of investigations connected with Cu-C (multiwall carbon nanotubes (MWNTs), graphene nanopowder (GNP), or thermally reduced graphene oxide (RGO)) composites, produced using the spark plasma sintering technique. The obtained composites are characterized by uniform distribution of a carbon phase and high relative density. Compared with pure copper, developed materials are characterized by similar thermal conductivity and much lower values of thermal expansion coefficient. The most promising materials to use as heat dissipation elements seems to be copper-based composites reinforced by carbon nanotubes (CNTs) and GNP.
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