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Thermal analysis in experimental verification t o theoretical prediction of the maximum I iiicrosegregation phenomenon in the peritectic alloys solidification has been applied. Satis-I'actory agreement has been obtained between some results of theoretical calculations and experimental ones. Usibility of the YTA-5 apparatus (original construction of the Baykov I nstitute of Metallurgy) t o detect quite small amounts of low-solidifying non-equilibrium ~)hases has been proved.

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