In this study, viscoelastic properties of polymeric composites were investigated through a nondestructive test (NDT) method based on longitudinal free vibration. First, three different polyester composites reinforced separately with carbon, glass, and hemp fibers, as well as, one polyester composite sample reinforced with poplar wood powder were manufactured via pultrusion and hand lay-up methods, respectively. In the proposed resonant free vibration non-destructive method, each rodshaped test specimen was hit by a hammer at one end of specimen and immediately the acoustic response of the specimen was recorded by a microphone at the other end of the sample. Subsequently, the recorded sounds were analysed using fast Fourier transform technique. Then, frequency of the first mode of vibration for each composite specimen was utilised to calculate modulus of elasticity. Further, decrement in vibration energy as a function of time was examined to obtain loss parameter (tan d) of the provided composites. Moreover, parameters (i.e., elastic modulus and tan d) were also compared with those determined by dynamic mechanical thermal analysis (DMTA). It is found that the results obtained from the examined nondestructive test method are in consistent with those measured by DMTA approach, providing reliable, accurate and quick responses.
In many applications, viscoelastic properties of reinforced composites need to be determined prior to their real service life. Such properties can be assured by destructive and non-destructive tests. In this paper, a novel non-destructive test (NDT) method based on flexural free vibration is introduced to investigate the viscoelastic properties of fiber-reinforced composites. Three different types of industrial fibers (carbon, glass, and hemp) and an unsaturated polyester resin were selected to produce barshaped composites via pultrusion technique. These composite bars were used in a simple NDT method which just required a wooden hammer, two elastic jaws, a microphone and a recorder software program to perform the experiment. The composite bars were mounted on elastic jaws and hit by a wooden hammer at one end of the specimen as a perpendicular impulse. The produced sound at the other side of the bars was recorded. By analyzing the recorded sounds by means of fast Fourier transform (FFT), viscoelastic properties such as flexural elastic modulus and the loss parameter (Tan d) were calculated for the fiber-reinforced composites. For determination of flexural elastic modulus, the first three modes of vibration in FFT graphs were analyzed using Temuschenco theory. Also, Tan d was determined by analyzing the drop in the intensity of vibrational energy as a function of time. Although there was a slight discrepancy between the calculated values from the NDT method and the actual data from dynamic mechanical thermal analysis (DMTA) approach, a good agreement was achieved between NDT and DMTA results.
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