This paper describes a method of laser synthesis of titanium microspheres, titanium carbide and silicon oxide. The formation of microspheres is carried out under the action of femtosecond laser radiation on the surface of the sample. The analysis was carried out on a scanning electron microscope. The obtained titanium and titanium carbide microspheres have an average size of the main fraction of 1-3 μm and can be used in applications of additive technologies and powder metallurgy as the main raw material or as an alloying additive. The main fraction of silicon oxide granules lies in the range of 50-300 nm. To improve the efficiency of the particle output, a combined method of laser action and electric current is proposed.

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The influence of the chemical composition of the substrate material on the chemical and phase composition of the formed coating was investigated. A number of experiments aimed at studying the interaction of titanium alloys with ultrashort laser pulses in different reaction media was carried out. A new method for the formation of titanium carbide under the action of ultrashort laser pulses on the surface of a titanium sample in a liquid hydrocarbon and liquid nitrogen medium is described. The description of the experiment is presented. The treated surface was investigated using a scanning electron microscope. Raman spectra from the surface of treated titanium alloys under different exposure conditions are obtained.