This paper studies the electroless (Ni-P) deposition which is used in different engineering applications due to their ability to modify and enhance the surface properties of the steel substrate. The electroless plating process was used to prepare (Ni-Cu-P), (Ni-P) and (Ni-Cu-P/Nano TiO2) alloys in this research. Deposition process parameters based on (L28) Taguchi orthogonal configuration with three process parameters, viz., stirring speed, temperature, time, are designed for optimum microhardness. Under the Taguchi series, the microhardness activity of electroless (Ni-P-TiO2) nanocomposite deposition was measured. The findings revealed that the integration of TiO2 into the coating allows micro-hardness cause an increase. Finally, optimum conditions were achieved as A2B1C2 (i.e. Speed of stirring = 1000 r.p.m, Temperature = 90 °C and Time = 70 min).

The purpose of this study is designate quenching and tempering heat treatment by using Taguchi technique to determine optimal factors of heat treatment (austenitizing temperature, percentage of nanoparticles, type of base media, nanoparticles type and soaking time) for increasing hardness, wear rate and impact energy properties of 420 martensitic stainless steel. An (L18) orthogonal array was chosen for the design of experiment. The optimum process parameters were determined by using signal-to-noise ratio (larger is better) criterion for hardness and impact energy while (Smaller is better) criterion was for the wear rate. The importance levels of process parameters that effect on hardness, wear rate and impact energy properties were obtained by using analysis of variance which applied with the help of (Minitab18) software. The variables of quenching heat treatment were austenitizing temperature (985 C˚,1060 C˚),a soaking times (50,70 and 90 minutes) respectively, Percentage of volumetric fractions of nanoparticles with three different levels(0.01, 0.03 and 0.08 %) were prepared by dispersing nanoparticles that are  (α-Al2O3,TiO2 and CuO) with base fluids (De-ionized water, salt solution and engine oil).The specimens were tempered at 700°C after quenching of nanofluids for  (2 hours).The results for ( S/N) ratios showed the order of the factors in terms of the proportion of their effect on hardness, and wear rate  properties as follow: Austenitizing temperature ( 1060 C˚),Type of base media (salt solution), Nanoparticles type (CuO), Percentage of nanoparticles (0.08%) and Soaking time(90min) was the least influence while for the impact energy were as follows: Type of base media (oil), Austenitizing temperature (985C˚), Percentage of nanoparticles (0.01%), Nanoparticles type (α-Al2O3) and last soaking time (50min).

The current work is conducting an experimental investigation into the effect of those technical parameters, called nanomaterial, bath temperature and plating time on the micro-hardness and corrosion rate of electroless plated low carbon steel undergoing electroless deposition operation. It was used to prepare (Ni-P/ Nano TiO2), (Ni-P/ Nano Al2O3) and (Ni -P/ Nano SiO2) alloys in this research. The Taguchi design is used to describe the variations located within the corrosion and mechanical properties. To achieve a comprehensive study, a Taguchi-based design was used to account for all applicable combinations of factors. Experimental models had been advanced that linking the response and method parameters to the results of those experiments. Validation of these models is done using analysis of variance (ANOVA). The desirability function is used to simultaneously optimize all the response. Finally, the optimum combination of method parameters resulting (bath temperature=90 oC, plating time =120 min.  and Nanomaterial=(Al2O3)), nanomaterial was observed to be the major process parameter on the responses of the electroless-plated low carbon steel with an impact ratio of (47%) based on the (ANOVA) results.

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