This is a repository copy of Concentration profiling of a horizontal sedimentation tank utilising a bespoke acoustic backscatter array and CFD simulations.

No abstract

The aim of this study was to understand the efficacy of widely available minerals as dual-function adsorbers and weighter materials, for the removal of toxic azo-type textile dyes when combined with coprecipitation processes. Specifically, the adsorption of an anionic direct dye was measured on various mineral types with and without the secondary coagulation of iron hydroxide (‘FeOOH’) in both a bench-scale stirred tank, as well as an innovative agitated tubular reactor (ATR). Talc, calcite and modified bentonite were all able to remove 90–95% of the dye at 100 and 200 ppm concentrations, where the kinetics were fitted to a pseudo second-order rate model and adsorption was rapid (<30 min). Physical characterisation of the composite mineral-FeOOH sludges was also completed through particle size and sedimentation measurements, as well as elemental scanning electron microscopy to determine the homogeneity of the minerals in the coagulated structure. Removal of >99% of the dye was achieved for all the coagulated systems, where additionally, they produced significantly enhanced settling rates and bed compression. The greatest settling rate (9 mm min−1) and solids content increase (450% w/w) were observed for the calcium carbonate system, which also displayed the most homogenous distribution. This system was selected for scale-up and benchmarking in the ATR. Dye removal and sediment dispersion in the ATR were enhanced with respect to the bench scale tests, although lower settling rates were observed due to the relatively high shear rate of the agitator. Overall, results highlight the applicability of these cost-effective minerals as both dye adsorbers and sludge separation modifiers to accelerate settling and compression in textile water treatment. Additionally, the work indicates the suitability of the ATR as a flexible, modular alternative to traditional stirred tank reactors.

Abstract-Real time in situ characterisation of solids concentration would aid operational understanding and improve efficiency in many industrial systems. This is especially true in the processing of legacy nuclear wastes where hazardous material is encountered. Acoustic methods have been previously demonstrated for the measurement of concentration in solid-liquid systems at a small scale. This study explores the use of the ultrasound array research platform (UARP) for backscatter measurements of concentration at a large scale in a dynamic settling system. The theory of acoustic measurement of solids concentration is described for both backscatter based attenuation and backscatter power methods. Acoustic based backscatter power and attenuation measurements are compared to laboratory analysed samples. Ultrasonic solids concentration analysis is shown to reveal flow dynamics within the settling tank.