The purpose of this study was to evaluate the ability of three resin composite systems to mask a severely discolored background by the application of a layering technique through CIELAB and CIEDE2000 analysis. Ninety 1.5-mm-thick disc specimens were produced from three different resin composite restoration systems: IPS Empress Direct (Ivoclar Vivadent), Charisma Diamond (Heraeus Kulzer), and Filtek Z350 XT (3M-ESPE). The specimens were divided into groups according to the restoration system and the resin composite shade combination used for the layering technique (enamel, body, and dentin shades). Color measurements were performed by a reflectance spectrophotometer (SP60, EX-Rite) against a C4 shade background and an inherent color background, which simulates a severely discolored background and a tooth surface with no discoloration, respectively. The total color difference between both color measurements was calculated by CIELAB (ΔE*) and CIEDE2000 (ΔE) formulas. The mean ΔE* and ΔE values were analyzed by analysis of variance (general linear models) and Tukey's post hoc tests (α=0.05). Three groups presented clinically acceptable color difference values (ΔE*≦3.46 and ΔE≦2.25): 1.5 mm dentin, 1.0 mm dentin/0.5 mm body, and 1.0 mm dentin/0.5 mm enamel; ie, all the groups from the Z350 XT restoration system. The resin composite layering technique is an effective way to mask severely discolored backgrounds. The Filtek Z350 XT system was the only restoration system capable of masking the C4 background.

SUMMARY The aim of this study was to evaluate the effectiveness of the layering technique to mask a discolored background (C4) after one year of water aging. The technique was used with three resin composite restorative systems (IPS Empress Direct, Charisma Diamond, and Filtek Z350XT). Ninety 1.5-mm-thick specimens were divided into groups and subgroups according to the restorative system and resin composite shade combination used in the layering technique (enamel, body, and dentin). The color measurements were made by reflection spectrophotometer (SP60, EX-Rite) over the C4 substrate at two time points: after 24-hour water immersion (T0) and after one-year water aging (T1). The masking ability was evaluated by calculating the ΔE between an inherent color background and a C4 background at T0 and T1. CIELAB and CIEDE2000 formulas were used for comparative analysis between T0 and T1 color measurements. Analysis of variance and Turkey's post hoc test (a=0.05) were performed to analyze ΔEab and ΔE00 mean values. The Z350XT restorative system presented adequate masking ability in the combinations of 0.5 mm body + 1.0 mm dentin, 0.5 mm enamel + 1.0 mm dentin, and 1.5 mm dentin after 24-hour water immersion. The masking ability was affected negatively by water aging in most of the combinations. The IPS Empress Direct was the only system that remained stable after aging in the combinations of 0.5 mm enamel + 1.0 mm dentin and + 1.5 mm dentin (p=0.05 and p=0.47 for CIELAB; p=0.15 and p=0.51 for CIEDE2000), although it did not present adequate masking ability in both time points. None of the combinations of any system presented adequate masking ability after prolonged water aging.

Objectives:To evaluate the effects of dentin pretreatment and temperature on the bond strength of a universal adhesive system to dentin.Material and Methods:Ninety-six extracted non-carious human third molars were randomly divided into 12 groups (n=8) according to Scotchbond Universal Adhesive (SbU) applied in self-etch (SE) and etch-and-rinse (ER) mode, adhesive temperature (20°C or 37°C) and sodium bicarbonate or aluminum oxide air abrasion. After composite build up, bonded sticks with cross-sectional area of 1 mm2 were obtained to evaluate the microtensile bond strength (μTBS). The specimens were tested at a crosshead speed of 0.5 mm/min on a testing machine until failure. Fractured specimens were analyzed under stereomicroscope to determine the failure patterns in adhesive, cohesive (dentin or resin) and mixed fractures. The microtensile bond strength data was analyzed using two-way ANOVA and Tukey's test (α=5%).Results:Interaction between treatment and temperature was statistically significant for SbU applied in self-etch technique. Both dentin treatments showed higher bond strength for ER mode, regardless of adhesive temperature. When compared to control group, sodium bicarbonate increased bond strength of SbU in SE technique. Adhesive temperature did not significantly affect the μTBS of tested groups. Predominantly, adhesive failure was observed for all groups.Conclusions:Dentin surface treatment with sodium bicarbonate air abrasion improves bond strength of SbU, irrespective of adhesive application mode, which makes this approach an alternative to increase adhesive performance of Scotchbond Universal Adhesive to dentin.

Clinical Relevance Conventional multistep resin cements presented higher adhesive performance to dentin than simplified self-adhesive cements, which is an important criterion for indirect restoration prognosis.

The use of acid etchants to produce surface demineralization and collagen network exposure, allowing adhesive monomers interdiffusion and consequently the formation of a hybrid layer, has been considered the most efficient mechanism of dentin bonding. The aim of this study was to compare the tensile bond strength to dentin of three adhesive systems, two self-etching ones (Clearfil SE Bond -CSEB and One Up Bond F -OUBF) and one total-etching one (Single Bond -SB), under three dentinal substrate conditions (wet, dry and re-wet). Ninety human, freshly extracted third molars were sectioned at the occlusal surface to remove enamel and to form a flat dentin wall. The specimens were restored with composite resin (Filtek Z250) and submitted to tensile bond strength testing (TBS) in an MTS 810. The data were submitted to two-way ANOVA and Tukey's test (p = 0.05). Wet dentin presented the highest TBS values for SB and CSEB. Dry dentin and re-wet produced significantly lower TBS values when using SB. OUBF was not affected by the different conditions of the dentin substrate, producing similar TBS values regardless of the surface pretreatments. Descriptors: Dentin permeability; Dentin-bonding agents; Tensile strength.Resumo: O uso de condicionadores ácidos para desmineralizar a superfície dental e expor a rede de fibras colágenas para interdifusão dos monômeros adesivos e conseqüente formação da camada híbrida tem sido considerado o mais eficiente mecanismo de adesão dos agentes de união. O objetivo deste estudo foi comparar a resistência de união à dentina de três sistemas adesivos, dois autocondicionantes (Clearfil SE Bond -CSEB e One Up Bond F -OUBF) e um de condicionamento total (Single Bond -SB), sob três diferentes condições de substrato dentinário (úmido, seco e reidratado). Noventa terceiros molares humanos recém-extraídos foram cortados na superfície oclusal, para se remover o esmalte e formar uma parede plana de dentina. Os espécimes foram restaurados com resina composta (Filtek Z250) e submetidos ao teste de resistência de união à tração (TBS) em uma MTS 810. As médias foram submetidas à ANOVA a dois critérios e ao teste de Tukey (p = 0,05). A dentina úmida apresentou os maiores valores de TBS para os sistemas adesivos SB e CSEB. A dentina seca e a reidratada apresentaram TBS significativamente menor quando foi empregado SB. OUBF não apresentou resultados influenciados pela condição do substrato dentinário, tendo produzido TBS similares para os diferentes tratamentos de superfície. Descritores: Permeabilidade da dentina; Adesivos dentinários; Resistência à tração.