Schiff-oxime ligands characterized by the existence and participation of iminic-and oximic azomethine groups in coordination with metal ions [1-3]. Metal complexes of imineoxime have various applications in different scientific fields. It has been used as antimicrobial [4], antibacterial [5], antifungal [5,6] as well as anticancer [7]. Some of Schiff oxime derivatives have been used in extraction [8] and spectrophotometric determination [9] of metal ions. Imine-oxime complexes have been also found used as catalysts for selective oxidation of alcohols to ketones and aldehydes [10]. EXPERIMENTAL Chemicals have been procured from Fluka and Sigma-Aldrich. Shimadzu (FT-IR), 4800S spectrophotometer has been used to get FTIR spectra of prepared compounds (4000-400 cm-1 , KBr). Cary 100con. spectrophotometer has been used for electronic spectra of prepared compounds at wavelength 200-800 nm. Stuart digital SMP30 apparatus used for measuring melting points of compounds. Mass spectrum of H2L was performed on GC-MS QP-2010 (Shimadzu). NMR spectra of H2L in DMSO-d6 were recorded by Bruker DMX-500 spectrophotometer (300 MHz). Phoenix-986 AA spectrophotometer has been used to estimate the metal ions percentages.