Recent archaeomagnetic studies carried out on Mid-to Late Holocene burnt anthropogenic cave sediments have shown that under certain conditions, these materials are suitable geomagnetic field recorders. Archaeomagnetic analyses carried out on these contexts constitute a rich source of information not only for geophysical purposes-in terms of reconstructing the variation of Earth's magnetic field in the past-but also from the archaeological point of view, for example by archaeomagnetic dating. Here, we report three different archaeomagnetic applications to the study of burnt cave sediments: (i) archaeomagnetic dating; (ii) determining palaeotemperatures and (iii) assessing postdepositional processes. The first case study is a dating attempt carried out on a Late Holocene (Bronze Age) burnt level from El Mirador Cave (Burgos, Spain). Using the directional European secular variation curve, several dating intervals were obtained for the last burning of this combustion feature. Considering the archaeological evidence and the independent radiometric (14 C) dating available the possible ages obtained are discussed. This is the first archaeomagnetic dating obtained in these contexts so far. The second case study is an application of the method to determine the last heating temperatures reached by the carbonaceous facies of these fires. Stepwise thermal demagnetization of oriented samples can be used to quantitatively estimate heating temperatures. An intermediate normal polarity component interpreted as a partial *Manuscript Click here to view linked References 2 thermo-remanence (pTRM) with maximum unblocking temperatures of 400-450 ºC was systematically identified, revealing the last heating temperatures experienced by this facies. These temperatures were confirmed with partial thermomagnetic curve experiments. Finally, archaeomagnetic analyses on a partially bioturbated burning event were performed in order to evaluate until what spatial extent the burnt sediments were affected by post-depositional mechanical alteration processes. For each case study, the archaeological implications are discussed highlighting the potential of archaeomagnetic methods to retrieve archaeological information.
Summary An archaeomagnetic, rock magnetic and magnetic fabric study has been carried out on seven anthropogenic ash horizons in the Middle Paleolithic sedimentary level XXIV at the rock shelter of Crvena Stijena (‘Red Rock’), Montenegro. The study has multiple goals, including the identification of iron bearing minerals formed during combustion, assessment of the suitability of these combustion features for recording the Earth´s magnetic field direction, revelation of the magnetic fabric and its significance in the characterization of cave (rock shelter) burnt facies, and identification of post-burning alteration processes. Magnetite has been identified as the main ferromagnetic component of the ash. The ash layers exhibit a high thermomagnetic reversibility in contrast to the irreversible behavior of their subjacent burnt black layers which is related to the different temperatures attained. Seven mean archaeomagnetic directions were obtained with acceptable statistical values indicating that these features recorded the field direction at the time of burning. However, some of them are out of the expected range of secular variation for mid-latitude regions suggesting post-burning alterations. The magnetic fabric of the ash was characterized by anisotropy of low field magnetic susceptibility measurements. Statistical analysis (box and whisker plot) of the basic anisotropy parameters, such as foliation, lineation, degree of anisotropy and the shape parameter, along with the alignment of the principal susceptibilities on stereoplots, revealed variation among the ash units. The diverse, oblate to prolate, lineated or strongly foliated, quasi-horizontally and vertically oriented fabrics of the units may indicate different slope processes, such as orientation by gravity, solifluction, run-off water, quasi-vertical migration of groundwater and post-burning/post-depositional alteration of the fabric by rockfall impact. In sum, the magnetic characterization of the ash layers has shown the occurrence of different post-burning alteration processes previously not identified at the site. Alteration processes in prehistoric combustion features are often identified from macroscopic observations but our study demonstrates that multiple processes can affect them and are usually unnoticed because they take place on a microscopic scale. Their identification is critical for a correct chronological and cultural interpretation of a site (e.g.: collection of samples for dating, stratigraphic displacement of remains), especially if significant alterations are involved. Magnetic methods are therefore a powerful but underutilized tool in paleolithic research for the identification and evaluation of taphonomic processes affecting prehistoric fires.
Archaeomagnetic and rock-magnetic methods are of great value in the identification of archaeological fire, especially in Palaeolithic sites where evidence is usually scarce, ambiguous or poorly preserved. Although taphonomic processes can significantly modify Palaeolithic combustion structures, the extent to which such processes affect the magnetic record remains unknown. Here we report the results of an archaeomagnetic study involving five, two-to-five-year-old experimental combustion structures in open-air and cave settings. Some of these combustion structures involved post-combustion human actions such as trampling and relighting. Our results show pseudo-single domain (PSD) magnetite as the main magnetic carrier. Wood ash layers of combustion structures are the most magnetic facies followed by thermally altered sediments constituting the combustion substrates. A decreasing magnetic concentration pattern in depth was observed as a function of temperature. Positive correlation was found between good-quality directional data and macroscopically well-preserved combustion structures. Partial thermoremanent magnetization (pTRM) was the main magnetization mechanism identified in the combustion substrate facies. These data coupled with partial thermomagnetic curve experiments show the potential of these methods to estimate maximum temperatures of the last combustion event. Relightings show very good directional results, but they cannot be identified because the time between them is not enough to statistically distinguish directional variations of the local Earth´s magnetic field. The substrate sediment of an intensively trampled combustion structure yielded reliable archaeomagnetic directions. The results are discussed in terms of magnetization preservation potential and the effects of taphonomic processes on the archaeomagnetic record.
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