Three new water-responsive luminescent lanthanide-free polyoxometalate (Ln-free POM) materials Na7[SbW6O24], K5Na2[SbW6O24] and K7[SbW6O24] were prepared by thermally dehydrating the known compounds Na7[SbW6O24]·16H2O, K5Na2[SbW6O24]·12H2O, and a new one K7[SbW6O24]·6H2O. The isostructural...
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