We present measurements of the magnetization hysteresis on neutron-and proton-irradiated YBa2Cu307 z single crystals. The crystals were irradiated to Auences of 2X 10' n cm (E")0. 1 MeV) and 1X10' p cm (E~=3.5 MeV), respectively. The magnetization was measured for both field directions. We observed increases of the hysteresis by a factor of 5 at 10 K and 1 T for H~~c for the neutronirradiated sample and a factor of 9 for the proton-irradiated sample. For H~~ab the hysteresis increased by a factor of 8 and 6, respectively. The irradiated crystals were annealed at 100, 200, and 300'C in air for 8 h each. The irradiation-induced decrease of T, is fully recovered after the final annealing step for both types of irradiation. The magnetization hysteresis for H~~ab decreases almost to its preirradiation level after annealing at 300'C for both types of irradiation. In contrast, for H~~c, 50% of the initial neutron-irradiationand 30% of the proton-irradiation-induced enhancements of the magnetization hysteresis are still maintained after the final annealing. The differences in annealing between neutron-and proton-irradiated samples are attributed to the different amount of point defects created by these types of irradiation.
Results of dc magnetization on neutron (n) -irradiated YBa2Cu307 q single crystals are presented.The crystals were irradiated to a fluence of 2X10' nlcm (E &0.1 MeV). The magnetization has been measured at 10, 40, and 70 K for both field orientations. The magnetization is thereby obtained by cooling the sample in zero field to the desired temperature. Then the field is ramped in steps of 0.25 T up to 5 T and reversed in the same steps. At each field the magnetization is measured. The hysteresis hM is defined as the difference in magnetization between descending and ascending branches in the hysteresis loop. At 10 K, we observe an increase of the hysteresis by a factor of 3 for H~~c and by a factor of 10 for H~~a, b due to n irradiation. After irradiation, some of the crystals were annealed at 100, 200, and 300'C for 8 h each. After each annealing step, the critical current densities and the transition temperatures were determined again. We observe that following the 300'C annealing, the magnetization hysteresis for H~~a, b is almost reduced to the preirradiation level (a reduction in J, of 90%), in contrast to the H~~c case, in which the decrease in hysteresis due to annealing is much less (a reduction in J, of 30%). Crystals irradiated under the same conditions were used for transmission-electron-microscopy (TEM) studies.By comparison between TEM and magnetization measurements, the role of the cascade defects in pinning was determined. It is furthermore shown by TEM that the cascade defects do not anneal for comparable annealing temperatures. We find that the hysteresis for H~~c is governed by both the cascade defects which do not anneal and point defects or their clusters on the Y layers or Cu02 planes which do anneal, whereas for H~~a, b, pinning is determined by oxygen defects in the CuO chains which anneal due to oxygen diffusion.
Magnetization and critical field measurements were carried out on a high-purity LaAl2 single crystal (RRR = 830) in the temperature range from 80 mK to the transition temperature (Tc=3.301 K). The material was identified to be a type-II superconductor with κ(Tc)=0.75±0.01 and µ0Hc2(0)=92.04 mT. As expected from the magnitude of κ, evidence for a first-order phase transition at Hcl is found. Experiments on the anisotropy of Hc2 in the (100)-plane show a field modulation of about 1% at 2 K. A complete evaluation of superconductive parameters will be presented.
Absrruct--We present the results of magnetization hysteresis and Tc measurements of neutron and proton irradiated YBaCuO single crystals. The crystals used for comparison were irradiated to a fluence of 2~1 0 '~n / c m~ (n, E>O.lMeV) and 1x1016p/cm2 @, Ek3.5MeV). The critical currents at 1T and 10K are enhanced by a factor of 5 for the neutron irradiated and a factor of 9 for the proton irradiated sample respectively. After irradiation the crystals were annealed at 100, 200 and 300°C for 8h each in air. Following each annealing step the critical temperature and the magnetization hysteresis at 10 and 70K was measured. Upon annealing, we observe a decrease of the critical currents, which is more pronounced for the proton irradiated sample. This decrease is related to the removal of point defects or their small clusters. Thus, their contribution to pinning can be studied. The critical temperature decreases after both types of irradiation by about 0.5K and is fully recovered after annealing.
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