Green synthesis of nanoparticles is rapidly evolving because it is cost-effective and eco-friendly, this also contributes to its preference over nanoparticles from other sources. In this study, silver nanoparticles were synthesized from Allium cepa (AC) and Raphanus sativus (RS) aqueous extracts and the biological activities were evaluated. The silver nanoparticles AgNPs@AC and AgNPS@RS were synthesized from AC and RS extracts, respectively, using silver nitrate and characterized using UV–visible spectroscopy (UV–Vis), Fourier transform infrared (FT-IR) spectroscopy, Powder X-ray diffraction (PXRD), scanning electron microscope (SEM) and energy dispersive X-ray spectroscopy (EDX). The FT-IR spectra of AgNPs@AC and AgNPS@RS showed characteristic groups pertaining to active molecules of the respective extracts indicating their surface functionalization. The XRD pattern of AgNPs@AC revealed diffraction peaks at 38.26, 44.39, 64.65, 77.54 and 81.64 that were indexed to (1 1 1), (2 0 0), (2 2 0), (3 1 1) and (2 2 2) planes of face-centered cubic (FCC) crystalline structure, respectively. The XRD pattern of AgNPs@RS revealed diffraction peaks at 38.24, 44.32, 64.62, 77.46 and 81.65 that was indexed to (1 1 1), (2 0 0), (2 2 0), (3 1 1) and (2 2 2) planes of face-centered cubic (FCC) crystalline structure, respectively. The SEM images indicate that the particles are spherical in shape and have particle size in the range of 25–35[Formula: see text]nm. The nanoparticles demonstrated substantial antimicrobial activity against Gram [Formula: see text]ve and Gram [Formula: see text]ve harmful bacteria species, such as S. aureus, E. coli and fungal species C. albicans. This study shows that A. cepa (Onion) and R. sativus (Radish) aqueous extracts can be used as an effective reducing and capping agent for the green synthesis of silver nanoparticles (AgNP). AgNPS@RS showed acceptable size and shape of nanoparticles and could therefore be a potential source of antimicrobial agents.
Copper nanoparticles (CuNPs) have captivated amazing and renewable interest in recent years due to their fascinating features. In present
investigation, CuNPs were produced by reducing copper sulphate with ascorbic acid (vitamin C) in aqueous medium without inert gas
insulation at low temperature (80 ºC). In present synthetic procedure, a native vitamin C was applied as insulating agent to prevent
oxidation of nascent CuNPs during the process and in storage. Triton X-100 was added that worked both as a size controller and as a
capping agent. The CuNPs were characterized by UV-visible and FT-IR spectroscopies, powder X-ray diffraction (PXRD) and scanning
electron microscopy-energy dispersive spectroscopy (SEM-EDX). Optical properties of Cu nanoparticles were explored using UV-vis
spectroscopy. FT IR was employed to uncover the bonding between copper nanoparticles and Triton X-100. The CuNPs were discerned
by PXRD and SEM-EDX Techniques. From the major diffraction peaks, the average particle size is determined using Debye-Scherer
equation and it is found to be about 15 nm. It is hoped that the present results would pave a way for developing plans for the production
of nascent CuNPs in the absence of inert gas insulation.
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