To improve the controllability of the fabrication of carbon aerogels, the effects of the concentration of the reactant (RF%) on the structural properties of organic resorcinol formaldehyde (RF) gel and the effects of the carbonization temperature on nanostructure of carbon aerogels were discussed. The concentration of the reaction was turned from 5%,10%,20%,30%,40%,50%,55% and 60% to prepare the samples. The RF aerogels were carbonized at temperature of 700, 900 and 1050. The shrinkage and nitrogen gas adsorption were measured. Experimental results showed that the structural stability of the organic RF aerogel can be improved by decreasing the shrink in drying process and increasing the condensation of reactant in the starting solution to a certain value, such as 55%. The ordered pore size distribution of carbon aerogels with less structure defects is able to be produced through the effective particle fusing at the carbonization temperature as high as 1050.
In this experiment UDP450 was used to prepare the CrAlTiN films with different Y contents deposited on Si(100) substrates. The thickness and structure of CrAlTiN films were characterized by scanning electron microscopy (SEM). The results show that the thickness of CrAlTiN films increases with the increasing of Y contents in Al targets. Meanwhile, the structures of these films are column structures with the least changes. XPS and EDS results indicate that Al contents in the films also increased with the increasing of Y contents in Al targets. Voltages of Al targets were changed with the variation of Y contents in Al targets when CrAlTiN layers were formed. The current of Al targets was a constant during producing CrAlTiN layer. The original voltages of Al targets during forming CrAlTiN layers increased greatly with the increase of Y contents in Al targets. The results show that the collision probability between the neutral particles and positive ions increased in the vacuum chamber. This indicates that the sputtering yield of Al targets is increased at a higher voltage. Consequently, the growing speed of CrAlTiN film and the sputtering yield of Al targets are all improved with the addition of Y element.
LiFePO4/C is synthesized via sol-gel method using Fe3+ as iron sources and complexing agents, followed by sintering at high temperature for crystallization. The amount of carbon in these composites is less than 6.8 wt.% and the XRD experiment confirms that all samples are pure single phase indexed with orthorhombic Pnma space group. The particle size of the LiFePO4/C synthesized by acetic acid as complexing agent is drastically fine with 200nm. The electrochemical performance of this material, including reversible capacity, cycle number and charge-discharge characteristics, exhibits better.
The objective of this study was to research the influence of the sweet sorghum straw fermented by the Compound Microbial Agent on the milk yield and milk composition of the cows. The results indicated that sweet sorghum straw bio-feed fermented by the Compound Microbial Agent in bags could increase the feed intake (11.4%) and milk yield(14.2%) compared with the control group, it also has improved milk protein (14.03%) and butterfat rate (16.3%) ,and has reduced the somatic cell's number(5.15%) compared with the control group. The sweet sorghum straw fermented by the Compound Microbial Agent has reduced the milk-feed ratio (20.8%).It has improved the feed digestibility and utilization and reduced the costing.
Magnesium alloy slurry was prepared using Strain-Induced Melt Activation(SIMA) technique. The samples were quenched into water so as to fix the high temperature instantaneous microstructures. The microstructure evolution of compressed deformation Mg alloy is studied in the process of continuous heating and iso-temperature of semi-solid state. The results indicate that deformed Mg alloy (AZ91) has first occurred to have the conversion of dendrite crystal-oriented isometric crystals in the continuous heating process. When the temperature rises to the range of semisolid state, the region with high energy at the pressed stripes begins to melt, showing that the cellular structures emerge in the crystal boundary and melting micro-pool phenomena appear within the crystals. With the iso-temperature time in semisolid state prolongs, the isometric crystals can be gradually converted into spherical crystal grains.
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