NiO/ZnO nanocomposites synthesized by sol-gel method with zinc chloride and nickel nitrate hexahydrate in ethanol used as solvent. Material was characterized by Particle size analyzer, UV-Vis, FTIR, TGA and DSC. NiO/ZnO nanoparticles investigated as a suitable photocatalytic material for the methylene blue degradation i.e. an organic dye under visible light irradiation. The UV–vis absorption spectra of the NiO/ZnO nanoparticles shown peaks in the UV region, corresponding to the band gap of the NiO/ZnO nanoparticles. The band gap of NiO/ZnO nanoparticles is calculated 3.55 eV by Tauc’s plot method. Then UV visible data showed the methylene blue degradation with NiO/ZnO nanoparticles, behaving as active catalyst.

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Ethylene glycol is solvent used in sol-gel method to synthesize NiO/ZnO nanocomposites. ZnCl2 along with NiCl2.6H2O were used as precursors during synthetization of NiO/ZnO nanocomposites. We used various techniques such as Thermogravimetric Analysis (TGA), Differential Scanning Calorimetry (DSC), Fourier Transform Infrared Spectroscopy (FTIR) and particle size analysis for synthesis of the nanocomposites which confirm that these nanocomposites act as catalyst.

T he nanoparticles play a significant role in fabrication process which are used at large scale in various fields e.g., sensors, electronics drug delivery, optics, catalysis and in water purification process. Nanoparticles (NiO/ZnO) were synthesized using sol-gel technique. In this method, 2-propanol was taken to analyze the particle size. Fourier Transform Infrared Spectroscopy (FT-IR) confirmed the presence of ZnO/NiO. Ultraviolet Visible (UV) data recorded a band gap for ZnO that was 4.1 eV while UV spectrum of methylene blue demonstrated a decrease in concentration of methylene blue while using NiO/ ZnO as catalyst.

The nanoparticles play a significant role in fabrication process which are used at large scale in various fields e.g., sensors, electronics drug delivery, optics, catalysis and in water purification process. Nanoparticles (NiO/ZnO) were synthesized using solgel technique. In this method, 2-propanol was taken to analyze the particle size. Fourier Transform Infrared Spectroscopy (FT-IR) confirmed the presence of ZnO/NiO. Ultraviolet Visible (UV) data recorded a band gap for ZnO that was 4.1 eV while UV spectrum of methylene blue demonstrated a decrease in concentration of methylene blue while using NiO/ ZnO as catalyst.