This study evaluated the effect of extending the duration of exposure to curing light on the depth of cure of two conventional (RBC1‐conventional and RBC2‐conventional) and two bulk‐fill (RBC1‐bulk and RBC2‐bulk) resin composites. Polywave and single‐peak photocuring units were used. Cylinder‐shaped specimens were exposed to curing light either for the time period recommended by the manufacturer or twice the length of that time, and depth of cure was estimated using manual scraping (similar to the ISO‐4049 standard) and solvent immersion techniques. Depth of cure was analyzed, using two‐way ANOVA, for the factors measurement method and exposure time. For RBC1‐conventional and RBC1‐bulk, the solvent immersion technique estimated a greater depth of cure than did manual scraping; for RBC1‐conventional, both techniques and both light‐exposure time periods resulted in a depth of cure of >2 mm; and for RBC1‐bulk, only the solvent method after photocuring for twice the manufacturer’s recommended time resulted in a depth of cure of 5 mm. For RBC2‐conventional and RBC2‐bulk, neither technique nor exposure time resulted in estimated depths of cure that matched those indicated by the manufacturer. The results suggest that extending the duration of photopolymerization increases depth of cure. Also, calculation of depth of cure can vary according to the measurement technique used.
The objective of this study was to compare two methods to evaluate the depth of cure (DOC) of restorative composites and if the extension of the light-activation time would increase the DOC of composites.Two bulk-fill composites (Tetric Evoceram Bulk Fill, Ivoclar Vivadent and Filtek One Bulk Fill, 3M Oral Care) and two conventional composites (Tetric N-Ceram, Ivoclar Vivadent e Filtek Z350 XT, 3M Oral Care) were tested. Cylindrical samples were made by inserting the composites into a hole of matriz with 5 mm internal diameter and 13 mm depth, and light-activated with light curing unit from the same manufacturers of each composite, using the manufacturer recommendation time (MRT), or for double the time (DOT). Two methods compared were: 1-ISO 4049 test and 2-dissolution with organic solvent (acetone). For the ISO 4049 test, the unpolymerized resin was manually removed with a plastic spatula and the length of the samples measured with a digital caliper to calculate the DOC. In the organic solvent method, the unpolymerized resin was removed manually and samples were immersed inn the dark in acetone for 48 hours for DOC measurement. It was observed that light curing for DOT produced significantly higher DOC than those for MRT. Differences in DOC measurements between ISO and "organic solvent" methods were material dependent.
To evaluate the microtensile bond strength (µTBS) of two resin cements to 3D printed and milled CAD/CAM resins used for provisional fixed partial dentures. Blocks (5 x 5 x 5 mm) of three 3D-printed resins (Cosmos3DTemp / Yller; Resilab3D Temp / Wilcos and SmartPrint BioTemp, / MMTech) were printed (Photon, Anycubic Technology Co.). A milled material (VitaCAD-Temp, VITA) was used as control. Half the specimens were sandblasted and the rest were untreated. Two blocks were bonded with the corresponding resin cement: PanaviaV5 (Kuraray Noritake) and RelyX Ultimate (3M Oral Care). After 24 hours, the bonded blocks were sectioned into 1 x 1 mm side sticks. Half the beams were tested for µTBS and the other half was thermocycled (5000 cycles, 30s dwell-time, 5s transfer time) before µTBS testing. A four way Generalized Linear Model (material*sandblasting*cement*aging) analysis was applied. VITA exhibited the lowest µTBS, regardless of the cement, sandblasting and thermocycling. Sandblasting significantly improved the µTBS of VIT, especially after aging, but did not improve the µTBS of 3D printed resins. Sandblasting was not beneficial for 3D printed resins, although is crucial for adhesive cementation of milled temporary resins. Airborne particle abrasion affects the integrity of 3D-printed resins, without producing a benefit on the microtensile bond strength of these materials. However, sandblasting is crucial to achieve a high bond strength on milled temporary resins.
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