RESUMO Neste estudo, apresentam-se resultados do perfil logaritmo do vento, coletados no CLA durante cinco dias no mês de setembro de 2008. Os resultados mostram que o comprimento de rugosidade é da ordem de 0,4 m e a velocidade de fricção é aproximadamente 10% da velocidade do vento a 70 m. O perfil do vento obtido em uma torre anemométrica de 70 m com seis níveis de medições ajustam-se bem na forma logarítmica.
ZrO2(Y2O3)-based ceramics with coloring gradient can facilitate the development of dental prosthesis by the improvement of esthetic properties. In this work, ZrO2 powders with different particle sizes were investigated. White and yellow zirconia powders (TOSOH Corporation-Japan) were characterized by particles size distribution using nanoSight-LM20 analyzer. Furthermore, samples were characterized by X-Ray diffraction, Scanning Electron Microscopy and relative density. Compacts with two layers, one white and one yellow were uniaxially pressed at 80MPa and sintered at 1530°C-120min. The yellow-powder presented average particles size of 180±66nm, while the white-powder presented particles size of 198±73nm. After sintering, full dense ceramics with tetragonal phase were obtained. The linear shrinkage of the yellow and white-layer was 22.75% and 22.05% respectively. This difference in shrinkage is important in the machining of prostheses in ceramic CAD/CAM systems, because they lead to difficulties in adapting this customized prosthesis in patients.
In this work, the preparation of Al2O3-TiO2 ceramics by high-energy ball milling varying the molar fraction in 1:1 and 3:1 was investigated. The powder mixtures were processed in a planetary mill at 250rpm and a ball-to-powder weight ratio of 5:1, for 120min. Compacts were obtained by cold pressing at 100MPa. These specimens were heated at 1000◦C for 30min to promote the water evaporation, and subsequently sintered at 1500◦C for 240min. Samples were characterized by relative density and X-ray diffraction. Hardness and fracture toughness were determined by Vickers Indentation Method. The crystallite sizes were lower than 420 and 560Å in Al2O3-TiO2 and 3Al2O3-TiO2 powders, respectively. After sintering, XRD analysis indicates Al2TiO5 and Al2O3/Al2TiO5 as major crystalline phases for Al2O3-TiO2 and 3Al2O3-TiO2 compositions, respectively. The relative density of the Al2O3-TiO2 ceramics was higher than 90% in both compositions. However, hardness and fracture toughness results of 10.7GPa or 10.5GPa and 3.2MPa.m1/2 or 2.6MPa.m1/2 for Al2O3-TiO2 and 3Al2O3-TiO2 mixtures respectively, indicates that microstructure duplex composed by Al2O3 and Al2TiO5 grains lead to improvement of toughness of these ceramics.
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