A synthesis of a new dental material, based on nano‐structured highly active calcium silicates and calcium carbonates, is described in this paper. Phase analysis of this material, before and after hydration, was performed by X‐ray diffraction and showed that active silicate phases were transformed into tobermorite phase, while carbonates remained unchanged. The mechanism of hydration was fully described. The morphology of the sample was studied by SEM, and typical appearance of the present phases was particularly discussed. The mechanical properties and setting time of this material make it very promising for potential application in dental practice.
Objectives
To explore whether the commercial agents recommended for controlling dental biofilm formation had a significant effect in vivo on mechanical and corrosion properties of nickel-titanium (NiTi) alloy.
Materials and Methods
NiTi archwires (dimensions 0.508 × 0.508 mm) were collected from 36 orthodontic patients aged 13–42 years after a 3-month intraoral exposure. Three experimental groups were formed: (1) subjects conducting regular oral hygiene, (2) subjects who used fluorides for intensive prophylaxis for the first month, and (3) subjects who used chlorhexidine in the same manner. Corrosion behavior, surface characteristics, stiffness, hardness, and friction were analyzed.
Results
Exposure to intraoral conditions significantly reduced the stiffness and hardness of the NiTi alloy (P ≤ .015). Fluoride tended to reduce stiffness and hardness more than did saliva or antiseptic, but not significantly. Roughness and friction were not significantly influenced by oral exposure. Intraoral aging predominantly produced general corrosion independent of the adjuvant prophylactic agent, although localized corrosion may also have occurred.
Conclusions
Fluorides and the antiseptic chlorhexidine do not increase corrosion more than saliva itself, nor do they further modify the mechanical properties of the NiTi alloy.
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