A new precursor technique for the carbothermal synthesis of nanocrystalline AlN powder has been developed. A precursor that contains an intimate mixture of nanocrystalline Al 2 O 3 and carbon has been synthesized by using a chemical pyrophoric reaction. The formation of AlN starts at 1473 K, and complete conversion has been observed at temperatures >1673 K. The synthesized AlN particles are nanocrystalline (<100 nm) in size.

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Al-2Mg-11TiO 2 composite was successfully prepared by the conventional vortex method. The macrostructural observation revealed columnar structure with rutile particles being distributed throughout the matrix in the form of agglomerates. Microstructural observation showed the presence of micro voids in the particle-enriched zone. Electrical resistivity measurement showed a phase transformation at 360°C, which was consistent during DSC studies due to the precipitation of TiAl 3 phase. As-cast composite was both hot rolled and cold rolled successfully to 50 and 40% reduction, respectively. The mechanical properties of the thermomechanically-worked composite were studied. From fractographic analysis, it was clear that the crack had nucleated at the particle/matrix interface and propagated through the matrix by microvoid coalescence. Ultimate tensile strength of cold worked composite was found to be better than the hot worked material.

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