In order to reach high composite repair strength, it is advisable to sandblast the polished composite surface with aluminum oxide. A hydrophobic intermediate agent should then be applied in order to prolong durability of the composite repair.
This study evaluated the effect of a warm (W) or cold (C) air-dry stream for solvent evaporation on the immediate (IM) and six-month (6M) resindentin bond strength (µTBS) and silver nitrate uptake pattern (SNU) of two-step etch-and-rinse adhesive system (Adper Single Bond [SB] and Prime & Bond 2.1 [PB]). The adhesives were applied on demineralized dentin surfaces and a warm or cold air-dry stream (10 seconds) was applied followed by light-activation (10 seconds). After 24-hours of water storage, the specimens were serially sectioned in the "x" and "y" directions to obtain bonded sticks around 0.8 mm 2 to be tested immediately or after six months of water storage. The specimens at each period were immersed in a 50% solution of silver nitrate, photodeveloped and analyzed by SEM for SNU.
Clinical RelevanceIn terms of silver nitrate uptake, the use of a warm air stream may improve bonding interface resistance to degradation over time. In terms of bond strength values, a warm air stream only improved the resin-dentin bond strengths of the ethanol/water-based system.
Laboratory ResearchHigher IM µTBS values were observed for SB under W conditions. Both adhesives showed reductions in µTBS after 6M in both air temperatures. Regarding SEM, a low silver nitrate uptake was observed in the W groups either in IM or 6M for both adhesives.
One of the reasons for resin-dentin degradation is poor polymerization of the adhesive layer. This study evaluated the effect of prolonged polymerization times on the immediate and 6-month resin-dentin bond strengths, silver nitrate uptake, and polymer quality of etch-and-rinse adhesives. Thirty extracted teeth were obtained, and a flat dentin surface was exposed on each tooth. Adhesives (Adper Single Bond 2 and One Step Plus) were applied to the dentin surface of these teeth and light-cured for 10, 20, or 40 s at 600 mW cm(-2) . Bonded sticks (0.6 mm(2) ) were tested in tension (0.5 mm min(-1) ) and analyzed, after immersion in 50% silver nitrate, using scanning electron microscopy. The polymer quality of adhesive films was evaluated using thermogravimetric analysis. Statistically higher bond strengths were observed for both adhesives when light-cured for 40 s. Degradation of dentin bonds occurred under all experimental conditions but it was less pronounced for adhesives light-cured for 40 s. Longer exposure times reduced silver nitrate uptake for Adper Single Bond 2. Solvent retention and the amount of residual monomer were statistically lower when both adhesives were light-cured for 40 s. Although longer exposure times than those recommended cannot prevent degradation of the dentin bonds, they can increase bond strength, probably because of the removal of an increased amount of solvent and the presence of a lower amount of residual monomer.
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