Abstract. The N-(2,6-diisopropylphenyl)-NЈ-benzoylthiourea ligand (shown as L) (1) was synthesized and characterized. Reactions of 1 with CuCl 2 and CuBr 2 afforded the monomeric L 2 CuCl (2) and dimeric [LBrCu(μ-L)] 2 (3), respectively, due to the reduction of Cu II . The reaction of 1 and CuCl gave the same product L 2 CuCl (2), while the treatment of 1 with CuBr led to the formation of a rare example
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