A synthetic procedure based on the 1,3-dipolar cycloaddition reactions of nitrile oxides and ethynylferrocene derived from ferrocene has been developed to synthesize new ferrocenyl-isoxazole derivatives. The stable solids were thoroughly characterized by 1 H NMR, FT-IR, and mass spectroscopy. The structure of (η 5 -C 5 H 5 ) Fe (η 5 -C 5 H 4 ) C 3 HNOC 6 H 4 CH 3 was determined by singlecrystal X-ray diffraction. The electrochemical behaviors of the synthesized ferrocenyl-isoxazole derivatives were also studied.

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