The effects of nitrogen and oxygen absorption on lattice expansion of Ti-6Al-4V have been investigated by high-temperature X-ray diffractometry. Experiments have been performed on stress-free powder for its high surface-volume ratio and to avoid possible effects on diffraction patterns due to texture change and recovery of defective structures induced by the measurement cycle at temperature. Cell parameters a and c, measured at increasing temperatures up to 600°C, show linear trends with different slopes. As temperature increases, the cell volume expands and the c/a ratio changes. This is due to both lattice thermal expansion and absorption of oxygen and nitrogen. Part of the gas remains entrapped in the metal after cooling to room temperature causing a residual lattice distortion. Results have been compared with literature data obtained in analogous tests performed on bulk Ti-6Al-4V alloy both in vacuum and in inert gas atmosphere.
This paper deals with carbon steel and stainless steel clad-plate properties. Cladding is performed by the submerged-arc welding (SAW) overlay process. Due to element diffusion (Fe, Cr, Ni, and Mn), a 1.5 mm wide diffusion layer is formed between the stainless steel and carbon steel interface of the cladded plate affecting corrosion resistance. Pitting resistance is evaluated by measuring the critical-pitting temperature (CPT), as described in the American Society for Testing and Materials (ASTM) G-48 standard test. Additionally, Huey immersion tests, in accordance with ASTM A262, Type C, are carried out to evaluate the intergranular corrosion resistance. Some hardness peaks are detected in microalloyed steel close to the molten interface line in the coarse-grained heat-affected zone (CGHAZ). Results show that stress-relieving treatments are not sufficient to avoid hardness peaks. The hardness peaks in the CGHAZ of the microalloyed steel disappear after quenching and tempering (Q and T).
The conventional heat-treatment standard for the industrial post hot-forging cycle of AA7050 is regulated by the AMS4333 and AMS2770N standards. An innovative method that aimed to improve toughness behavior in Al alloys has been developed and reported. The unconventional method introduces an intermediate warm working step between the solution treating and the final ageing treatment for the high resistance aluminum alloy AA7050. The results showed several benefits starting from the grain refinement to a more stable fracture toughness KIC behavior (with an appreciable higher value) without tensile property loss. A microstructural and precipitation state characterization provided elements for the initial understanding of these improvements in the macro-properties.
Well-defined heat-treatment guidelines are required to achieve the target mechanical properties in high-chromium steels for forgings. Moreover, for this class of materials, the microstructure evolution during heat treatment is not clearly understood. Thus, it is particularly important to assess the steel microstructure evolution during heat treatment, in order to promote the best microstructure. This will ascertain the safe use for long-term service. In this paper, different heat treatments are considered, and their effect on a 7% Cr steel for forging is reported. Results show that, following the high intrinsic steel hardenability, significative differences were not found versus the cooling-step treatment, although prior austenite grain size was significantly different. Moreover, retained austenite (RA) content is lower in double-tempered specimens after heat treatments at higher temperatures.
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