The microstructural evolution of Fe-0.2C-5Mn steel during intercritical annealing with holding time for up to 144 hours was examined by TEM and STEM. It was demonstrated by TEM that the martensite lath structure gradually transformed into a lamellar ferrite and austenite duplex structure. The partitioning of manganese from ferrite to austenite was found by STEM. Typical Kurdjumov-Sachs orientation relationship between austenite lath and ferrite lath was observed by electron back scattered diffraction (EBSD). Based on the analysis of the austenite lath thckening behavior, it was proposed that the Mn-partitioning in austenite dominated the microstructure evolution of the ultrafine lamellar ferrite and austenite duplex structure during annealing process.
In this study Quenching and Partitioning (Q&P) as proposed by Speer was applied to improve the ductility of C-Mn high strength Low Alloy steel (HSLAs). Microstructural observations revealed a multiphase microstructure including first martensite, fresh martensite and retained austenite in the Q&P processed steel. During tensile process, the austenite volume fraction gradually decreased with strain increasing, suggesting the phase transformation induced plasticity for the Q&P processed steel. Ultrahigh strength about 1300-1800MPa and tensile elongation about 20% were obtained after Q&P processing at specific conditions, which is significant higher than that of ~10% of conventional martensitic steel. The the product of tensile strength to total elongation increased from 25 to 35GPa% with increasing carbon content in studied steel. This improved mechanical properties were related to the ductility contribution from TRIP effects of the retained austenite and strength contribution from the hard martensitic matrix. At last it was turned out that the Q&P process is a promising way to produce ultrahigh strength steel with relative high ductility under tailored heat treatment conditions for different micro-alloyed carbon steel.
The advantages and disadvantages of the conventional hot stamping steel and the hot tamping technology were shortly reviewed. It was proposed that new type steel with relative low austenization temperature and air hardening ability should be designed and produced to overcome the surface oxidation and avoid the complexity of cooling system of the stamping dies. In this study, it was shown that the 3rd generation sheet steel with medium-Mn composition could be austenized and pressed at 700-750°C and air cooled into automobile parts with strength no less than 1.5GPa and ductility larger than 12%. This new steel and corresponding forming technology were called warm stamping technology, which overcomes the disadvantages of the conventional hot stamping steel. The fabrication trials of the automobile parts in the automobile industries were demonstrated with high strength and relative good ductility. It was concluded that the 3rd generation sheet steel and the warm stamping technology could be applied to replace the conventional hot stamping steel and conventional hot stamping technology in near future.
An 18Ni (C-250) maraging steel was successfully processed by equal channel angular pressing (ECAP) for a single pass at room temperature. Microstructural observations showed that the martensite laths of 18Ni maraging steel were elongated to more narrow bands with a width of 100-200 nm after ECAP deformation. After ageing treatment, many nano-sized precipitates distributed uniformly within the refined martensite lathes. In comparison with the tensile strength (1940 MPa) of general used steel (solution + aging treatment), the tensile strength of the sample processed by ECAP and subsequent aging treatment was enhanced for more than 100 MPa (above 2050 MPa). The enhancement of tensile properties was attributed to microstructural refinement and uniformly distributed nano-precipitates.
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