A new vacuum system for the preparation of graphite samples for radiocarbon (14C) measurement using an accelerator mass spectrometer (AMS) was constructed at the Dendrochronological Laboratory in AGH-UST Kraków. The central part of the system is a manual vacuum line for the production of graphite from carbon dioxide for subsequent AMS measurements. The graphitization system can handle up to five samples simultaneously, and the process lasts for approximately 1 hour. The graphitization line was built to support the preparation of wood samples for a project dedicated to dating a subfossil tree from the Younger Dryas period. For this purpose, the chemical preparation procedure for wood samples was optimized to obtain more reliable results. This includes the extraction of α-cellulose to increase the precision of the age determination. The performance of the system was tested with NIST OxII, IAEA standards (IAEA C3, C5, C6, and C8), and background samples. The results of the 13 samples of subfossil wood were tested and are presented. The methodology gives good reproducibility of results obtained for the samples prepared using this system.
Miyake et al. (2012, 2013, 2014) described a sudden increase of radiocarbon (14C) concentration in annual tree rings of Japanese cedar (Cryptomeria japonica) and Hinoki cypress (Chamaecyparis obtusa) between AD 774 and 775 and between AD 993 and 994. In both analyzed periods, the sudden increase was observed almost in a single year. The increase in the 14C content was about 12‰ in the period AD 774–775 (Miyake et al. 2012) and about 11.3‰ in the period AD 993–994 (Miyake et al. 2013, 2014; Fogtmann-Schultz et al. 2017; Rakowski et al. 2018). A similar increase was observed in 660 BC, with a peak height of about 10‰ (Park et al. 2017). Single-year samples of dendrochronologically dated tree rings of deciduous oak (Quercus robur) from Grabie, a village near Krakow (SE Poland), spanning the years 670–652 BC, were collected and their 14C content was measured using an AMS technique. The results clearly show a rapid increase in the 14C concentration in tree rings around 660 BC similar to this observed in Park et al. (2017).
Radiocarbon (14C) analyses are commonly used to determine the absolute age of floating tree-ring chronologies. At best, with the wiggle-matching method, a precision of 10 years could be achieved. For the early Middle Ages, this situation has been markedly improved by the discovery of rapid changes in atmospheric 14C concentrations in tree-rings dated to 774/775 and 993/994 AD. These high-resolution changes can be used to secure other floating tree-ring sequences to within 1-year accuracy. While a number of studies have used the 774 even to secure floating tree-ring sequences, the less abrupt 993 event has not been so well utilized. This study dates a floating pine chronology from Ujście in Wielkopolska (Greater Poland) (NW Poland), which covers the 10th century period and is critical for studies on the beginning of the Polish State to the calendar years 859–1085 AD using the changes in single year radiocarbon around 993/4 AD.
Our dendrogeomorphological analysis was completed for 4 landslides, situated in the municipality of Węgierska Górka in the Beskid Śląski Mountains in Southern Poland. The local landslides pose a direct threat to the newly designed S-69 expressway running through the north-western part of the municipality. The research material consisted of 127 samples, collected with the use of a Pressler increment borer, from three species of coniferous trees (Norway spruce, Scots pine, and Silver fir). The landslide activity periods were identified on the basis of the splitting of the dendrochronological curves representing the upslope and downslope parts of the tree trunks. The largest number of the studied trees indicated reactions to substrate mass movements in 1964, 1971, 1972, 1984, 1994, 1997, 1998, and 2010. The detailed locations of the sampled trees allowed us to reconstruct the activities of particular landslide sections in time. We identified the fact that parts of the landslides located downslope of the planned road S-69 are more active than parts of the same landslides located above it on the slope. Geological conditions in the studied area favour landslide activity while precipitation is the main triggering factor of landslides.
Subfossil trunks of pine (Pinus sylvestris L.) from the Late Weichselian were discovered in the site Koźmin in the Koło Basin, central Poland (Dzieduszyńska et al., 2014a). Another part of organic sediments with trunks was excavated in the frame of the research project. Altogether 224 samples from Koźmin were analysed dendrochronologically; they represented generally young trees, 40 to 70 years old. Based on the most convergent sequences, the chronology 2KOL_A1 was produced, 210 years in length. With the wiggle-matching method, it was dated to ca. 13065–12855 cal BP. Dendrochronological dating of trunks buried in organic sediments, most of which occurred in situ, revealed that tree deaths occurred successively, over more than 100 years. That could have been due to unfavourable climatic conditions, as well as extreme events, e.g. strong winds.
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