In the present study, a method based on sulfuric acid dehydration of sugar was developed to synthesis a precursor material, which can yield B4C/ TiB2 composites at much lower temperatures compared to traditional carbothermal methods. The precursor material for pure B4C and B4C / TiB2 composites were heat treated at 1650oC under Ar and Ar+H2 atmosphere. Then the samples were characterized by X-ray diffraction (XRD) and crystallized B4C and B4C / TiB2 composites can be obtained at 1650oC

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