T he creep behaviour and the microstructural evolution of a 9Cr-Mo-Nb-V (T 91) steel were extensively evaluated by means of short term constant load creep tests and T EM analysis. Statistical analysis of the microstructural data revealed that the precipitated phases M 23 C 6 (where M is a metal, mainly Cr or Fe) and MX (where M is Nb or V, and X is C and/or N) were subject to coarsening during creep exposure. T he coarsening law and its dependence on applied stress were identified, and the model was used to predict the magnitude of the Orowan stress at the time corresponding to the minimum creep rate. T he minimum creep rate dependence on applied stress at 873 K was described by incorporating the threshold stress concept in a power law with stress exponent n=5. In the resulting phenomenological model, the strengthening eVect of the dispersed phases was thus expressed by a threshold stress proportional to the Orowan stress.MST /4310
In the present study, AlSi10Mg samples produced by selective laser melting (SLM) were studied. Samples were machined from two types of bars obtained through different methods: either single laser (SL) or multiple laser (ML) machine setup. The bars were built perpendicular to the platform, which was pre-heated at 150 °C (working temperature), up to a height of 300 mm. The effect of the distance from the platform on the mechanical properties was investigated through tensile samples in as-built condition and after unconventional heat treatments (U-HT). Tensile strength changed by 80 MPa along the Z-axis (build direction) for SL case and by 100 MPa for ML case in the as-built samples. Vickers microhardness revealed an analogous gradient. This was correlated to a gradient in intra-granular precipitates' distribution along the Z-axis, as revealed by scanning electron microscopy (SEM). An unconventional heat treatment at 175 °C for 6h slightly improves the mechanical strength; higher temperature treatments at 200 and 225 °C for the same duration cause a progressive decrease in strength with an increase in elongation. The amount and size of the precipitates and the thickness of eutectic Si change with the heat treatment temperature, justifying the mechanical behavior.
Laser powder bed fusion (L-PBF) is an additive manufacturing technology that is gaining increasing interest in aerospace, automotive and biomedical applications due to the possibility of processing lightweight alloys such as AlSi10Mg and Ti6Al4V. Both these alloys have microstructures and mechanical properties that are strictly related to the type of heat treatment applied after the L-PBF process. The present review aimed to summarize the state of the art in terms of the microstructural morphology and consequent mechanical performance of these materials after different heat treatments. While optimization of the post-process heat treatment is key to obtaining excellent mechanical properties, the first requirement is to manufacture high quality and fully dense samples. Therefore, effects induced by the L-PBF process parameters and build platform temperatures were also summarized. In addition, effects induced by stress relief, annealing, solution, artificial and direct aging, hot isostatic pressing, and mixed heat treatments were reviewed for AlSi10Mg and Ti6AlV samples, highlighting variations in microstructure and corrosion resistance and consequent fracture mechanisms.
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