This research was based on the manufacture of new composite materials that offer technological possibilities in the development of new devices with greater efficiency. Electrospinning was used to form nylon 66/-tetra-(para-aminophenyl) porphyrin (H 2 T(p-NH 2 )PP)/graphene oxide (GO) composite film. Graphene oxide coatings were obtained from graphite, through mechanical exfoliation followed by calcination and ultrasonic agitation in an oxidant solution. These samples were characterized under SEM, FTIR, Raman spectroscopy, UV-vis and R-X techniques.

In this work, synthesis and characterization of reduced graphene oxide/polyaniline/Au nanoparticles (GO/PANI/NpAu) as a hybrid capacitor are presented. Graphite oxide (GO) was synthesized by a modified Hummer's method. Polyaniline was synthesized by chemical polymerization, and Au nanoparticles (NpAu) were added afterward. Fabrication of the electrodes consisted on the hybrid materials being deposited on carbon cloth electrodes. The chemical and structural properties of the electrode were characterized by high-resolution scanning electron microscopy (HRSEM), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (X-R), and Raman spectroscopy; the results confirm the graphene reduction, the covalent functionalization, and formation of nanocomposites and also show the polyaniline grafted graphene. The performance and evaluation of the electrodes based on grapheme oxide (GO), polyaniline (PANI), GO-PANI, and GO/PANI/NpAu nanocomposites over carbon cloth, stainless steel, and copper have been obtained in 1 M H 2 SO 4 solution, using electrochemical techniques namely: cyclic voltammetry (CV) and electrochemical impedance spectroscopy (EIS). They showed that GO/PANI/NpAu gave higher specific capacitance (SC) and energy values than PANI, and GO/PANI, in the order of 160 F/g. The present study introduces new hybrid material for energy applications, from the evaluation of their electrical contributions.