In the past years a wide discussion has been held among asphalt researchers regarding the existence and interpretation of observed microstructures on bitumen surfaces. To investigate this, the RILEM technical committee on nano bituminous materials 231-NBM has conducted a round robin study combining differential scanning calorimetry (DSC) and Atomic Force Microscopy (AFM). From this, methods for performing DSC and AFM tests on bitumen samples and determination of the influence of wax on the observed phases, taking into account thermal history, sample preparation and annealing procedure, are presented and critically discussed. DSC is used to measure various properties and phenomena that indicate physical changes such as glass transition temperature (T g) and phase transition such as melting and crystallization. In the case of existence of wax, either natural or synthetic, it can further indicate the melting point of wax, that could be used to determine wax content. The results from seven laboratories show

No abstract

No abstract

International audienceThe valorization of Scenedesmus sp. microalgae byproducts was investigated, as a potential route for the production of road binders from renewable sources. Under hydrothermal liquefaction conditions, a water-insoluble viscous material was obtained in a ca. 55% yield, which consists of an oily fatty acid-based fraction mixed with organic and inorganic solid residues (up to 22%). Although the chemical composition of the obtained materials completely differs from that of petroleum-based bitumen, similar viscoelastic properties were observed in some cases, depending on the hydrothermal liquefaction experimental conditions. A rheological simple material could thus be obtained, which compared well with a bitumen reference

No abstract