Cured and uncured scraps from manufacturing of epoxy based carbon fiber reinforced composites were treated with a pyrolytic process to provide, as solid residue, carbon fibers to be re-used in new composites production. The industrial scraps were pyrolyzed at different temperatures in a 70 kg batch pilot plant and the pyrolysis products (gas, oil, and solid) were fully characterized. The solid residue (carbon fibers covered by a carbonaceous layer) was subjected to a further oxidative step at 500 and 600 C for different residence times to provide fibers devoid of any organic residue that did not volatilize during pyrolysis. The effects of both pyrolysis and oxidative process on the recovered fibers were evaluated by scanning electron microscopy and Raman Spectroscopy. The reinforcement behavior of pyrolyzed and pyrolyzed/oxidized chopped fibers, compared to virgin fibers, was tested in the production of new Chopped Carbon Fiber Reinforced Composites. The optimized double pyrolysis/ oxidation process was found to provide fibers whose performance in the composites were comparable to the virgin ones. POLYM. COMPOS., 36:1084-1095, 2015
The diffraction capability of two crystalline silicon plates bent by carbon fiber deposition has been studied. The performed treatment induced a permanent curvature in the samples, resulting in an increase of the diffraction efficiency. The obtained efficiencies are constant over a wide angular range and close to the theoretical expectations, meaning that the curvatures were homogeneous. Most importantly, the bending technique allowed the manufacture of bent samples up to 5 mm thick and with a radius of curvature down to 30 m. With such a technique, the fabrication of crystals for the realization of a hard X-ray concentrator (Laue lens) for astrophysical purposes is enabled
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