In this study, the mechanical, antibacterial properties and cell toxicity response of Ti-5Al2.5Fe alloy with different copper contents were investigated. The alloys were prepared by high-energy ball milling using elemental Ti, Al, Fe, and Cu powders and consolidated by a uniaxial vacuum hot press. Staphylococcus aureus strain ATCC 29213 and Escherichia coli strain ATCC 25922 were used to determine the antibacterial properties of the sintered alloys. The in vitro cytotoxicity of the samples was evaluated with HeLa (ATTC, CCL-2) cells using thiazolyl blue tetrazolium bromide. The mechanical behavior of the samples was determined as a function of hardness and bending tests and analyzed by scanning electron microscopy, energy dispersive x-ray spectroscopy, optical microscopy and x-ray diffraction (XRD). The results showed that the Cu content significantly improved the antibacterial properties. Cu addition prevented the formation of E. coli and S. aureus colonies on the surface of the samples. All samples exhibited very good cell biocompatibility. The alloys with different copper contents showed different mechanical properties, and the results were correlated by microstructural and XRD analyses in detail. Our results showed that Cu has a great effect on the Ti5Al2.5Fe alloy and the alloy is suitable for biomedical applications with enhanced antibacterial activity.

In the current research, the effect of Ag on the mechanical properties of Ti5Al2.5Fe alloy was investigated. The Ti5Al2.5Fe alloy, with different amounts of Ag ranged from 1 to 5 wt. % was prepared by mechanical mixing and then fabricated by hot pressing at 950?C for 15 min under 50 MPa. Three holding steps were applied to the powder compacts to restrain the liquid phases inside graphite die before reaching the maximum sintering temperature. The sintered samples were subjected to hardness, bending and wear tests to study the effect Ag on the mechanical properties of Ti5Al2.5Fe alloy. The microstructural characterization was carried out by means of optical and scanning electron microscope. The results showed that Ag played a differential role on the mechanical properties supported by microstructural constituents. The bending strength and hardness of the produced samples increased with the addition of Ag, the hardness of the alloys then tended to decrease with increasing Ag content but still remained above the hardness of Ti5Al2.5Fe alloy. Wear test also showed similar trends with hardness test results. Finally, the optimum Ag content for the Ti5Al2.5Fe alloy was determined as 1 wt.%. XRD analysis showed that undissolved Ag content was the main reason for the decrease in the mechanical properties.

In the current study, hard facing nickel alloy powders were coated in situ on pure iron by uniaxial hot pressing under vacuum atmosphere to improve its hardness and wear properties. The nickel alloy powders were placed onto the iron powders within a graphite die and then sintered at 1000 °C under 40 MPa for 10 minutes. Hardness and wear properties were studied by using a Vickers hardness tester and a ball-on-disk tribometer, respectively. The wear rates of the samples were evaluated using a sliding velocity of 0.13 m × s−1 under normal loads of 20, 30, 40 and 50 N at room temperature. The interface layer between the nickel layer and pure iron substrate was also evaluated by scanning electron microscopy and energy dispersive spectroscopy. The results showed that sintered samples exhibited strong bonding at the interface. The hardness and wear properties of the materials increased effectively after nickel coating.

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Bu çalışmada saf alüminyum (Al) matris içerisine ağırlıkça % 0.25, 0.5 ve 1 oranlarında nano silisyum karbür partikülleri ilave edilmiş ve ardından toz karışımları önce mekanik alaşımlama, daha sonra sıcak pres ile sinterleme işlemine tabi tutulmuştur. Sinterleme sonrasında elde edilen numuneler metalografik işlemler ile hazırlanıp aşınma ve eğilme testlerine tabi tutulmuştur. Aşınma testleri sonucunda, saf Al matrise artan miktarda nanopartikül ilavesinin, belli orana kadar aşınma direncini arttırdığı gözlenmiştir. Benzer şekilde, artan nanopartikül takviyesiyle, eğilme testi sonuçlarında da gözle görülür artışın olduğu gözlenmiştir. Takviye partiküllerinin yapı içerisindeki dağılımını incelemek amacıyla numunelere EDX analizi ile elementel dağılım analizi yapılmıştır. Elde edilen sonuçlar literatür ile karşılaştırılarak değerlendirilmiştir.