The hydrogen content of free-standing polycrystalline CVD diamond samples was determined by Fourier Transform Infrared (FTIR) measurements and was quantified by a notched neutron spectrum technique. The latter measures the total bonded and unbonded hydrogen. The concentration of total hydrogen in these samples was of the same order of magnitude. The FTIR measurements, which are sensitive to the bonded hydrogen, indicated different hydrogen to diamond peak ratios.
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