Under different exploitive conditions, the humidity levels of the backfill stopes are not the same. Humidity greatly affects the strength and microscopic characterization of the backfill. Cemented paste backfill (CPB) specimens were cured using 0, 30, 70% and standard curing (20°C, 99%) under four different humidity conditions. At 28 days, nuclear magnetic resonance (NMR) and scanning electron microscopy (SEM) techniques were used to obtain the microscopic features of the CPB specimens. The relationships between the permeability and uniaxial compressive strength (UCS) of the CPB specimens, and the microscopic characteristics of the CPB specimens, were established. The results showed the following: (i) The permeability of the CPB had an exponential functional relationship with its stone powder content. (ii) The stone powder content of CPB and the peak area of the T2 spectrum are negatively correlated with the UCS. However, there was a T2 peak area corresponding to the worst UCS with the same stone powder content. (iii) The peak area of the T2 spectrum showed that the proportion of area of a small pore size was more than 80%, indicating that the pore size was mainly small. The pore diameter of small pores was linearly and inversely proportional to the UCS of the specimens. It can be found that the factors affecting the strength characteristics of CPB include not only the stone powder content, but also the curing conditions of different humidity.
Pore structure is a critical factor affecting the strength characteristics of mine backfill materials. In this paper, based on the mechanical tests on lime modified phosphogypsum cemented backfill (LMPGCB), the microstructure of the LMPGCB sample was characterized by nuclear magnetic resonance (NMR) and scanning electron microscopy (SEM) imaging. Based on the fractal theory (FT), the values expressing the fractal characteristics of the NMR T2 spectrum and SEM images were determined. The mathematical model between the NMR-FT fractal dimension and the SEM-FT box dimension was developed to infer the overall pore characteristics from various pore characteristics. The functional relationships between the strength and pore content and dimension were established, and the effects of pore structure on the strength were discussed. The results indicate that: (1) in NMR-FT fractal dimension, the fractal effect of various types of pores is better. The fractal dimension of the small pore is between 0.86–1.38, in which the overall trend first decreases and then increases. (2) In the SEM-FT box dimension, the fractal effect of the overall pore is better. The overall trend of box dimension decreased first and then increased at each kind of magnification. Furthermore, with the increase of magnification, the box dimension decreases. (3) There is a linear direct proportional relationship between the SEM-FT box dimension and the fractal dimensions of NMR-FT of small pores. The relationship between SEM-FT box dimension and NMR-FT fractal dimensions of various types of pores conforms to the plane relationship. There is a linearly increasing relationship between dimension and pore content and a decreasing relationship between dimension and strength.
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