In this study, the use of cotton fiber (CF) as a filler in poly(butylene succinate) (PBS) and the effect of silane treatment on the mechanical properties, thermal stability, and biodegradability of PBS/CF composites are investigated. The results showed that the tensile strength of PBS was improved (15%–78%) with the incorporation of CF (10–40 wt%) and was further increased (25%–118%) when CF was treated with a silane coupling agent. Scanning electron microscopy (SEM) observation of the fracture surfaces of PBS/CF composites showed that there was slight improvement in fiber-matrix compatibility. Thermogravimetric (TG) analysis showed that the thermal stability of the composites was lower than that of neat PBS and decreased with increasing filler loading. The biobased carbon content of the composites increased with increasing CF content. The incorporation of CF (with and without silane treatment) in PBS significantly increased the biodegradation rate of the composites
Anaerobic biodegradation tests of poly(lactic acid) (PLA) powder were done at the thermophilic (55 °C) and mesophilic temperature (35 °C) under aquatic conditions [total solid concentrations of the used sludge were 2.07% (at 55 °C) and 2.24% (at 35 °C)] using a newly developed evaluation system. With this system, the evolved biogas is collected in a gas sampling bag at atmospheric pressure. This method is more convenient than using a pressure transducer or inverted graduated cylinder submerged in water. PLA was degraded about 60% in 30 days, about 80% in 40 days and about 90% in 60 days at 55 °C. On the other hand, the PLA degradation started in 55 days at 35 °C and degradation rate was much slower than at 55 °C.
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