We report the complete GNO solar neutrino results for the measuring periods GNO III, GNO II, and GNO I. The result for GNO III (last 15 solar runs) is View the MathML source[54.3−9.3+9.9(stat)±2.3(syst)]SNU(1σ)(1σ) or View the MathML source[54.3−9.6+10.2(incl. syst)] SNU (1σ ) with errors combined. The GNO experiment is now terminated after altogether 58 solar exposure runs that were performed between 20 May 1998 and 9 April 2003. The combined result for GNO (I + II + III) is View the MathML source[62.9−5.3+5.5(stat)±2.5(syst)] SNU (1σ ) or View the MathML source[62.9−5.9+6.0] SNU (1σ ) with errors combined in quadrature. Overall, gallium based solar observations at LNGS (first in GALLEX, later in GNO) lasted from 14 May 1991 through 9 April 2003. The joint result from 123 runs in GNO and GALLEX is [69.3±5.5(incl. syst)] SNU[69.3±5.5(incl. syst)] SNU (1σ). The distribution of the individual run results is consistent with the hypothesis of a neutrino flux that is constant in time. Implications from the data in particle- and astrophysics are reiterated
We report the first GNO solar neutrino results for the measuring period GNO I, solar exposure time May 20, 1998 till January 12, 2000. In the present analysis, counting results for solar runs SR1–SR19 were used till April 4, 2000. With counting completed for all but the last 3 runs (SR17–SR19), the GNO I result is [65.8 ± 10.29.6 (stat.) ± 3.43.6 (syst.)] SNU (1σ) or [65.8 ± 10.710.2 (incl. syst.)] SNU (1σ) with errors combined. This may be compared to the result for Gallex (I–IV), which is [77.5 ± 7.67.8 (incl. syst.)] SNU (1σ). A combined result from both GNO I and Gallex (I–IV) together is [74.1 ± 6.76.8 (incl. syst.)] SNU (1σ)
Ca(OH)2 nanoparticles in hydro-alcoholic dispersion (nanolime) were successfully employed in Cultural Heritage conservation, thanks to the ability to overcome the limiting aspects of traditional lime treatments. Nanolime were currently produced by chemical precipitation process, at high temperature, with long times of synthesis, and after several purification steps to remove undesired secondary phases. In this paper, an innovative, simple and original method for nanolime production was described. The method was based on an ion exchange process between an anionic resin and a calcium chloride aqueous solution, operating at room temperature. A pure Ca(OH)2 nanoparticles suspension can be rapidly obtained after separating the resin from suspension, and any purification step was necessary. The exhausted resins can be regenerated and reused for a cyclic nanolime production. Structural and morphological features of the produced nanolime were preliminarily characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Moreover, XRD measurements allowed estimating nanoparticles reactivity by following their carbonatation process in air, in relation to different water/alcohol ratios and medium or high relative humidity conditions. The produced Ca(OH)2 nanoparticles appeared hexagonally plated, with dimension less than 100 nm and, compared with those obtained by typical wet precipitation method, they proved to be more reactive.
In this study, the conditions leading to the formation of cells and to the onset of crystallization of polycarbonate were examined with the use of supercritical carbon dioxide for the production of foams from preforms. Small plaques cut from extruded sheets were treated with supercritical carbon dioxide in an autoclave at temperatures varying from 60 to 200°C and from 4.5 to 30 MPa pressure. Visual observations and stereoscan electron microscopy examination revealed that penetration of supercritical carbon dioxide takes place via the advancing layer mechanism and that, for the particular grade of polycarbonate used in this study, the nucleation of the cells can take place at temperatures as low as 60°C. It requires, however, long treatment times and high pressures, and the growth of foam cells is severely restricted. Nucleation and growth of cells occurred much more readily at somewhat higher temperatures. With treatments at around 80°C, the onset of crystallization started to impose considerable hindrance to the formation of uniform and evenly distributed cells. This becomes increasingly evident at higher temperatures, between 100 and 180°C, owing to the formation of large spherulitic crystalline domains. A very effective nucleation and growth mechanism for the formation of cells was obtained, on the other hand, with treatments at 200°C due to the absence of crystallization phenomena. The degree of crystallinity increased with increasing treatment temperature, and the resulting morphology gave rise to two broad melting peaks. These are displaced to higher temperatures and become closer, merging into one peak with a low‐temperature shoulder. These events were monitored by thermal analysis and wide‐angle X‐ray diffraction examinations. © 2007 Wiley Periodicals, Inc. Adv Polym Techn 25:225–235, 2006; Published online in Wiley InterScience (http://www.interscience.wiley.com). DOI 10.1002/adv.20075
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