Nanocarbon-doped Fe-sheathed MgB 2 tapes with different doping levels were prepared by the in situ powder-in-tube method. Compared to the undoped tapes, J c for all the C-doped samples was enhanced by more than an order of magnitude in magnetic fields above 9 T. At 4.2 K, the transport J c for the 5 at% doped tapes reached 1.85×10 4 A/cm 2 at 10 T and 2.8×10 3 A/cm 2 at 14 T, respectively. Moreover, the critical temperature for the doped tapes decreased slightly. Transmission electron microscopy showed a number of intra-granular dislocations and the dispersed nanoparticles embedded within MgB 2 grains induced by the C doping. The mechanism for the enhancement of flux pinning is also discussed. These results indicate that powder-in-tube-processed MgB 2 tape is very promising for high-field applications.
We have successfully developed a 1020MHz (24.0T) NMR magnet, establishing the world's highest magnetic field in high resolution NMR superconducting magnets. The magnet is a series connection of LTS (low-Tc superconductors NbTi and Nb3Sn) outer coils and an HTS (high-Tc superconductor, Bi-2223) innermost coil, being operated at superfluid liquid helium temperature such as around 1.8K and in a driven-mode by an external DC power supply. The drift of the magnetic field was initially ±0.8ppm/10h without the (2)H lock operation; it was then stabilized to be less than 1ppb/10h by using an NMR internal lock operation. The full-width at half maximum of a (1)H spectrum taken for 1% CHCl3 in acetone-d6 was as low as 0.7Hz (0.7ppb), which was sufficient for solution NMR. On the contrary, the temporal field stability under the external lock operation for solid-state NMR was 170ppb/10h, sufficient for NMR measurements for quadrupolar nuclei such as (17)O; a (17)O NMR measurement for labeled tri-peptide clearly demonstrated the effect of high magnetic field on solid-state NMR spectra.
We report significant transport critical currents firstly achieved in Sr 0.6 K 0.4 Fe 2 As 2 wires and tapes with a T c = 34 K, which were fabricated through an in-situ powder-in-tube process. Silver was used as a chemical addition as well as a sheath material. Transport measurements were performed by a standard four-probe resistive method. All the wire and tape samples have shown transport properties. Critical current density J c was enhanced upon silver addition, and at 4.2 K, a best J c of ~1200 A/cm 2 (I c = 9 A) was achieved for 20 % silver added tapes, which is the highest in iron-based wires and tapes so far. The J c is almost field independent between 1 T and 10 T, exhibiting a strong vortex pinning. Such a high transport critical current density is attributed to the absence of reaction layer between the silver sheath and superconducting core, as well as an improved connectivity between grains. We also identify a weak-link behavior from the creep drop of J c at low fields and a hysteretic phenomenon. Finally, we found that compared to Fe, Ta and Nb tubes, Ag was the best sheath material for the fabrication of high-performance 122 type pnictide wires and tapes so far.
The world's largest pulsed superconducting coil was successfully tested by charging up to 13 T and 46 kA with a stored energy of 640 MJ. The ITER central solenoid (CS) model coil and CS insert coil were developed and fabricated through an international collaboration, and their cooldown and charging tests were successfully carried out by international test and operation teams. In pulsed charging tests, where the original goal was 0.4 T/s up to 13 T, the CS model coil and the CS insert coil achieved ramp rates to 13 T of 0.6 T/s and 1.2 T/s, respectively. In addition, the CS insert coil was charged and discharged 10 003 times in the 13 T background field of the CS model coil and no degradation of the operational temperature margin directly coming from this cyclic operation was observed. These test results fulfilled all the goals of CS model coil development by confirming the validity of the engineering design and demonstrating that the ITER coils can now be constructed with confidence.
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