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Objective:This study sought to assess the influence of cervical preflaring and reuse after resterilization, on fracture strength and plastic deformation and/or surface cracking in reciprocating nickel–titanium [NiTi] endodontic instruments after root canal instrumentation of extracted human teeth.Materials and Methods:Forty engine-driven reciprocating NiTi instruments (20 Reciproc® [RC], VDW; 20 WaveOne® [WO], Dentsply) were used in root canal instrumentation of extracted human molars. A total of 485 human upper molars with similar anatomical features were selected and randomly distributed across four groups according to the instrumentation procedures performed (G1 and G3: RC; G2 and G4: WO). Reciprocating instruments were used as per manufacturer instructions. In groups G3 and G4, cervical preflaring was performed prior to instrumentation. After each use of each instrument, sterilization was repeated and scanning electron microscope (SEM) images were obtained to check for plastic deformations and/or cracks on instrument surfaces. Each instrument was used repeatedly until fracture occurred.Results:Regardless of flaring, RC files exhibited greater fracture strength than WO instruments (P <0.01) with and without preflaring. Cervical preflaring significantly reduced the risk of instrument fracture (P <0.01). No plastic deformations were observed before fracturing. However, cracks were found on WO instruments shortly after their first use. RC and WO instruments resisted fracturing after autoclave sterilization.Conclusions:Cervical preflaring allowed a significant increase in the number of times RC and WO files could be reused safely.

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Stacking fault energy (SFE) is related to activating complex high strength and ductility mechanisms such as transformation-induced plasticity and twinning-induced plasticity effects. This type of energy can be estimated by many different methods and its importance is in its ability to predict microstructure and phase transformation behavior when the material is submitted to stress/strain. In order to study the SFE, chemical composition, and microstructure relationships, eleven different welding parameters were chosen to obtain a large range of dilution levels. A new tubular wire electrode of high-manganese steel (21 wt pct Mn) was used as the consumable and an SAE 1012 steel plate (0.6 wt pct Mn) as the base metal in a flux-cored arc welding process. These welding parameters were related to the phases formed and phase transformation behavior in the fusion zone. The SFE of the austenite phase was calculated using a thermodynamic model. The welding parameters produced SFE values in the range of À 5 to 7 mJ/m 2 . -martensite and austenite were observed in all samples, but a¢-martensite was only found in those that presented negative SFE values, i.e., those with lower Mn content. Chemical Gibbs Free energy was the component with the most influence on the SFE. Nanoindentation detected the phase transformations during hardness testing for the medium and low dilution levels used, while the high dilution levels presented the highest hardness and modulus of elasticity values, and the lowest elastic and plastic deformation values. The results provide an improved method to develop high-manganese steels with microstructure control through welding parameters.

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