Veröffentlicht in der Reihe Analytische Methoden zur Prüfung gesundheitsschädlicher Arbeitsstoffe: Analysen in biologischem Material , 11. Lieferung, Ausgabe 1994 Der Artikel enthält folgende Kapitel: Grundlage des Verfahrens Geräte, Chemikalien und Lösungen Geräte Chemikalien Lösungen Vergleichsstandards Probenahme und Probenaufbereitung Probenahme und Lagerung Extraktion der Organozinnverbindungen Extraktion des Gesamtzinns Atomabsorptionsspektrometrische Arbeitsbedingungen Analytische Bestimmung Kalibrierung und Berechnung des Analysenergebnisses Standardisierung der Meßergebnisse und Qualitätssicherung Beurteilung des Verfahrens Präzision Richtigkeit Nachweisgrenze Störeinflüsse Diskussion der Methode
Published in the series Analyses of Hazardous Substances in Biological Materials , Vol. 4 (1994) The article contains sections titled: General principles Equipment, chemicals and solutions Equipment Chemicals Solutions Calibration standards Specimen collection and sample preparation Specimen collection and storage Extraction of the organotin compounds Extraction of the total tin Operational parameters for atomic absorption spectrometry Analytical determination Calibration and calculation of the analytical result Standardization and quality control Reliability of the method Precision Accuracy Detection limit Sources of error Discussion of the method
Published in the series Analyses of Hazardous Substances in Air , Vol. 2 (1993) The article contains sections titled: General principles Equipment, chemicals and solutions Equipment Chemicals Solutions Sampling collection and preparation Cleaning of the equipment Conditioning of the exchange resin Preparation of the adsorption unit Sample collection and storage Sample preparation Operating conditions for atomic absorption spectrometry Atomic absorption spectrometry Pretreatment of the graphite tube Platforming technique Analytical determination and calibration Calculation of the analytical results Reliability of the method Precision Recovery rate Detection limit Sources of error Discussion of the method
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