We present accurate measurements of the triple point of nitrogen. The quality of this triple point is once more confirmed, and its temperature value is found to be T 90 = 63.152 6 K (expanded uncertainty U = 0.30 mK, reproducibility better than 0.1 mK). This is the first direct determination of this point on ITS-90 since the introduction of the scale. This point is useful as a non-uniqueness checkpoint.
Miniature glass and stainless-steel cells have been made at the
Institute of Low Temperature and Structure Research for the realization of the
triple point of mercury (T90 = 234.3156 K) to be used for the calibration
of capsule-type standard platinum resistance thermometers. This paper gives
details on the construction of these cells and some measurement results
obtained at the triple point of mercury.
In the temperature range from 0.65 K to 24.5561 K, the ITS-90 is defined by specified vapour-pressure equations for 3He and 4He and interpolation equations for a constant-volume gas thermometer using 3He or 4He. The definitions are given in sections 3.1 and 3.2 of the ITS-90 text, and methods for realising the scale in this range are outlined in chapters 4 and 5 of the Guide to the Realization of the ITS-90 (formerly Supplementary Information for the ITS-90). Direct realisations of the ITS-90 by these methods require relatively sophisticated apparatus and time-consuming experiments, and consequently they are rarely carried out. The situation is acceptable in practice only because rhodium-iron resistance thermometers (RIRTs) are available that, once calibrated, are able to maintain their calibrations reliably for long periods of time. They are the practical thermometers on which realisations of the ITS-90 are most accurately maintained, disseminated and compared. The key comparison EURAMET.T-K1 is therefore a comparison of calibrated RIRTs.
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