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In single crystals the NQR nutation frequency depends on the relative orientation of the coil and the quadrupole axes. In powders the nutation lineshape is a superposition of spectra from the randomly oriented single crystals, so that powder patterns appear in such experiments if the recon­struction is performed by the Fourier transform method. In this paper an alternative reconstruction method of nutation spectra is suggested making use of the Hankel Transform. In this way the nutation spectra are simplified. Singularities arising with experiments for the determination of the asymmetry parameter η can easily be resolved. In the particular case of an axially symmetric quadrupolar tensor and a homogeneous radiofrequency field one can reduce the powder pattern to a single line without heterogeneous broadening with respect to orientation. Further improvement o f the nutation spectra can be achieved by taking advantage of the maximum entropy method, which strongly reduces apodisation and noise problems. Applications of the new data manipulation techniques to N Q R imaging methods published elsewhere and 2D zero-field N Q R spectroscopy are reported.

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