This paper focuses on the Fe59.5Ni28Al11.5Ta1 memory alloy, in which the effects of different aging treatments on microstructure and properties of the rolled alloy are investigated by metallurgical microscope, X-ray diffraction, SEM, EDS and pressure test machine. Results show that, because of aging treatment, precipitation of γ’ and β’ phase strengthens the austenitic matrix. With the increase of aging time at 600 ℃, the comprehensive analysis of pseudoelasticity curve, shows that the stress-induced martensite critical stress of the aging state of the alloy decreases first and then increases; the alloy compressive strength, the recoverable strain and the hardness increase first and then decrease, Besides, the alloy residual strain is first decreased and then increased. When the aging time is 60 h, the alloy compressive strength is the maximum, up to 1306 MPa, the alloy recoverable deformation is the maximum, reaching 14.9%, the hardness of the alloy is also the largest, but the alloy residual strain is relative minimum. With the increase of aging time, alloy maximum strain decreases gradually, and the plasticity of the alloy also decreases gradually. The properties of the shape memory alloy are influenced by the particle size, its distribution, volume fraction, of precipitate phase etc.
To investigate an environmentally benign stabilizer for coarse-grained soil in southeast Tibet, poly (vinyl alcohol) (PVA) and silica fume were used to improve the geotechnical properties of coarse-grained soil. Unconfined compressive strength (UCS) and wet–dry cycle tests were conducted on prepared samples to evaluate the effect of the additive content and curing age on the strength and durability of coarse-grained soil. The results reveal that the UCS of the samples increased with the additive content of PVA solution and the curing age. The optimal value for the additive content of PVA solution and the curing age is 12% and 7 days, respectively. With the optimal PVA solution content, the PVA solution combined with silica fume stabilizer exhibited better reinforcement compared with pristine PVA. The UCS of the samples stabilized by PVA solution and silica fume increased depending on the curing age, and plateaued after 14 days. Samples with 12% PVA solution and 6% silica fume achieved a satisfactory UCS of 1543.17 kPa after curing for 28 days. As the number of wet–dry cycles increased, the UCS of the samples stabilized by the PVA solution and silica fume exhibited an upward trend during the first three wet–dry cycles, owing to the filling of pores by the gel produced by the silica fume, but began to decline as the number of wet–dry cycles increased. All samples retained a high UCS value after 10 wet-dry cycles compared with the samples that were not subjected to wet–dry cycles.
Materials with violent hydration reaction such as cement are used to solidify sandy soil slopes, which will cause destructive damage to the ecology of the slopes. In this paper, polyvinyl alcohol (PVA) and activated magnesium oxide (MgO) are used to improve sandy soil, and the effects of the dosage and curing age of modifiers on the mechanical properties of solidified sandy soil are studied. The dry–wet durability of the composite improved sandy soil is analyzed using a dry–wet cycle test, and the improvement mechanism of PVA and activated magnesium oxide is revealed using an electron microscope. The results show that the curing effect of polyvinyl alcohol and activated magnesium oxide on sand particles is better than that of polyvinyl alcohol alone. The compressive strength of improved soil samples increases with the increase of curing time, and magnesium oxide as an improved material needs appropriate reaction conditions to give full play to its role. The compressive strength of composite improved samples increases first and then decreases during the dry–wet cycle. Through the observation of microstructure, it can be seen that the cementing material wraps and connects the sand particles, and the cementing material of the sample after the dry–wet cycle develops more completely; if the magnesium oxide content is high, cracks may appear inside the sample.
Laboratory freezing experiments were conducted to evaluate the effect of polyacrylamide (PAM) and lignocellulose on the mechanical properties and microstructural characteristics of Tibetan clay. Direct shear and unconfined compressive tests and field emission scanning electron microscopy analyses were performed on clay samples with different contents of stabilizers. The test results show that the addition of PAM can improve the unconfined compressive strength and cohesion of Tibetan clay, but an excessive amount of PAM reduces the internal friction angle. After several freeze-thaw cycles, the unconfined compressive strength and cohesion of samples stabilized by PAM decrease significantly, while the internal friction angle increases. Samples stabilized by PAM and lignocellulose have higher internal friction angles, cohesion, and unconfined compressive strength and can retain about 80% of the original strength after 10 freeze-thaw cycles. PAM fills the pores between soil particles and provides adhesion. The addition of lignocellulose can form a network, restrict the expansion of pores caused by freeze-thaw cycles, and improve the integrity of PAM colloids. It is postulated that the addition of a composite stabilizer with a PAM content of 0.4% and a lignocellulose content of 2% may be a technically feasible method to increase the strength of Tibetan clay.
To improve the stability of sand slopes in Southeast Tibet, the wet–dry cycle test, immersion test, and permeability test were carried out using polyvinyl alcohol (PVA) as the improving material. The improvement effect was evaluated by considering the unconfined compressive strength. The results have revealed that the unconfined compressive strength of the improved soil significantly increased with the PVA content, while the degradation of the improved soil by wet–dry cycling and water immersion weakened. However, the permeability of the improved soil slightly decreased compared with that of unmodified soil. Through scanning electron microscopy (SEM), it was found that PVA only forms an elastic network structure in the sand to wind and connect the soil particles, but pores remain in the sand. This indicates that the addition of PVA does not affect the permeability to a great extent but greatly increases the strength. The findings of this study provide a useful reference for the practical application of PVA.
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