Objectives:The objective of this in vitro study was to evaluate the surface roughness and micro-hardness of three novel resin composites containing nanoparticles after polishing with one-step and conventional multi-step polishing systems.Methods:A total of 126 specimens (10 X 2 mm) were prepared in a metal mold using three nano-composites (Filtek Supreme XT, Ceram-X, and Grandio), 21 specimens of each resin composite for both tests (n=63 for each test). Following light curing, seven specimens from each group received no polishing treatment and served as controls for both tests. The specimens were randomly polished using PoGo and Sof-Lex systems for 30 seconds after being wet-ground with 1200-grit silicon carbide paper. The mean surface roughness of each polished specimen was determined with a profilometer. The microhardness was determined using a Vickers hardness measuring instrument with a 200-g load and 15 seconds dwell time. The data were analyzed using the Kruskal-Wallis test and the post hoc Dunn's multiple comparison tests at a significance level of .05.Results:Among all materials, the smoothest surfaces were obtained under a matrix strip (control) (P<.05). There were no statistically significant differences among polishing systems in the resin composites for surface roughness (P>.05). The lowest hardness values for the three resin composites were obtained with a matrix strip, and there was a statistically significant difference compared with other polishing systems (P<.05) whereas no statistically significant differences were observed between the polishing systems (P>.05).Conclusion:The current one-step polishing system appears to be as effective as multi-step systems and may be preferable for polishing resin composite restorations.
PURPOSEThe purpose of this study was to evaluate and compare the effects of different surface pretreatment techniques on the surface roughness and shear bond strength of a new self-adhering flowable composite resin for use with lithium disilicate-reinforced CAD/CAM ceramic material.MATERIALS AND METHODSA total of one hundred thirty lithium disilicate CAD/CAM ceramic plates with dimensions of 6 mm × 4 mm and 3 mm thick were prepared. Specimens were then assigned into five groups (n=26) as follows: untreated control, coating with 30 µm silica oxide particles (Cojet™ Sand), 9.6% hydrofluoric acid etching, Er:YAG laser irradiation, and grinding with a high-speed fine diamond bur. A self-adhering flowable composite resin (Vertise Flow) was applied onto the pre-treated ceramic plates using the Ultradent shear bond Teflon mold system. Surface roughness was measured by atomic force microscopy. Shear bond strength test were performed using a universal testing machine at a crosshead speed of 1 mm/min. Surface roughness data were analyzed by one-way ANOVA and the Tukey HSD tests. Shear bond strength test values were analyzed by Kruskal-Wallis and Mann-Whitney U tests at α=.05.RESULTSHydrofluoric acid etching and grinding with high-speed fine diamond bur produced significantly higher surface roughness than the other pretreatment groups (P<.05). Hydrofluoric acid etching and silica coating yielded the highest shear bond strength values (P<.001).CONCLUSIONSelf-adhering flowable composite resin used as repair composite resin exhibited very low bond strength irrespective of the surface pretreatments used.
Background
The aim of this study was to investigate the potential of concentrated fluoride varnishes to reduce enamel loss from repeated cycles of citric acid erosion and toothbrush abrasion in vitro.
Methods
Polished human enamel samples were exposed to fluoride varnishes: Bifluorid10® (NaF&CaF2‐ 45200 ppmF), Duraphat® (NaF 22600 ppmF), Fluor‐Protector® (difluorsilane 1000 ppmF) and a control coating of copal ether varnish (0 ppmF) group and a deionized water group. For each group of 16 samples, nine cycles of erosion and nine cycles of erosion‐abrasion [1 cycle = erosion (0.3% citric acid, pH 3.2, 5 min) + artificial saliva (1 h, pH 7.0) + abrasion (120 linear strokes in artificial saliva from Oral B medium soft brushes 300 g loading]. The change in the enamel surface was evaluated using optical profilometry.
Results
Duraphat® and Bifluorid10® applications had a median (IQR) step height of 4.21 um (1.59) and 5.01 um (1.02). This was statistically significantly less than Fluor‐Protector® 6.83 um (1.25), copal ether 7.22 um (1.97) and water 7.39 um (1.96) (p < 0.001). For erosion‐abrasion, both Duraphat® and Bifluorid® had statistically lower step heights than the other products (p < 0.01).
Conclusions
The action of fluoride in a range of single‐application topical varnishes was effective in reducing enamel wear from erosion and erosion‐abrasion in this laboratory study.
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