Many photochemical or photobiological applications require the use of high power ultraviolet light sources, such as high-pressure mercury arc lamps. In addition, many photo-induced chemical, biochemical and biological applications require either a combinatorial setting or a parallel assay of multiple samples under the same environmental conditions to ensure reproducibility. To achieve this, alternative, controllable light sources, such as ultraviolet light emitting diodes (UV LEDs) with high power and spatial control are required. Preferably, LEDs are arranged in a suitable standardized 96-well microtiter plate format. We designed such an array and established the methods required for heat management and enabling stable, controllable illumination over time.
Chemical adhesion promoters are necessary for the production of long-term stable metal-rubber composites. After these have been applied, rubber is molded onto the metallic base bodies by rubber injection molding. In (very) small batches, the adhesion promoter can be applied in precise volumes by hand using a fluid dispenser. However, this prevents homogeneity and uniformity of the layer thickness, which can cause variation in the reliability and strength of adhesion. As a technical solution, a pipetting robot has been envisaged. With the aid of several mechanical and electrical adaptations - including a new control technology - various fluid dispensers were integrated on 3-axis portal milling machines. Thus, full functionality could be achieved.
A passive pipe sampler device for contaminant analysis in groundwater was developed which create a permanent sampling flow from groundwater and in addition to temperature, conductivity and pressure, now also has room for specific sorbents. The large surface of the adsorber offers more binding surface for the analyte and the constant movement of the sorbent with fresh groundwater also provides homogeneous binding. The spectroscopic analyses at the monitoring site of the pipe passive sampler for groundwater monitoring points enables a measurement-based validation of the sorbent circulation as an alternative to a visual assessment. The optimum pump speed for the sorbens Lewatit® M500 and SR7 was evaluated. The 42mm slim measuring device allows the use in DN50 monitoring well and thus allows the setup of a closer measuring network.
The goal of this project was to enable an automated solution for the application of bonding agents to metallic bodies in the nanoliter range. For the automated application of adhesion promoters, a new control unit based on a mainboard for controlling 3D printers was used, with Marlin serving as the firmware. Adaptations were necessary in the area of motor currents, speeds, acceleration, sensitivity, print bed size and selection of mainboard and display. For the traverse paths, G-code was generated using a program in Python. For homogeneous and uniform wetting, the individual objects to be wetted are approached and the pipetting process is controlled. It was possible to establish the complete functionality.
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