High-pressure homogenizers are frequently employed for the homogenization of low-viscosity emulsions containing a proportion of disperse phase which is not too high. High-pressure homogenizers essentially consist of a high-pressure pump and a homogenizing nozzle. The design of the homogenizing nozzle influences the flow of the emulsion in the nozzle itself and hence the results of droplet disruption. It is shown which mechanism in frequently used homogenizing nozzles is usually responsible for disruption. Experimental results reveal the effects of the dispersed phase content and the viscosity of the disperse and continuous phases in different nozzles. The results can be explained on the basis of the mechanisms of disruption. Finally, the homogenizing nozzles presented are directly compared with one another.
Power ultrasound is one means among others of mechanically producing emulsions. In spite of numerous publications on the basic principles of this technique, there is insufficient knowledge of continuous ultrasound emulsification processes and the main parameters of practical relevance. A comparison of this system with other continuous mechanical emulsifying devices is made. The effect of continuous phase viscosity on droplet disruption due to ultrasound is the subject of a more detailed investigation. Continuous phase viscosity is varied by means of water soluble stabilizers (o/w systems) and different oils (w/o systems). At constant energy density, droplet size decreases when adding stabilizers, whereas the viscosity of the oil in w/o emulsions has no effect. Qualitative investigations of the local distribution of cavitation have shown very small penetration depths of cavitation into the liquid. This emphasizes the need for improvement of apparatus design to optimize the emulsification process.
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