Abstract. ZnO nanorods were successfully synthesized by the plasma torch with the zinc powder as the source of ZnO. Several testing was conducted to examine the results of ZnO nanoparticles among others are X-ray fluorescence (XRF), Scanning Electron Microscopy (SEM), and X-ray diffraction (XRD). The results of ZnO nanorods diameter vary from 87 nm to 263 nm which can be seen from SEM images and it is length varies from 300 to 1000 nm. It was found from XRD data that a sharp peak occured at 36.253º. It is indicated a good crystal growth and agreed well with the standard data (JCPDF-ICDD card no.: 36-1451). Effects of electrical current variations of plasma torch of 20, 25, and 30 Amperes on the size of ZnO nanorods are indicated from aspect ratio (72.85, 87.42, and 103 nm). The effects of electrical current of plasma torch on the purity of ZnO were about 95.61%, 98.46%, and 96.49% respectively. The performance of the solar cell at the time with the values of Voc, Jsc, FF, and efficiency are 0.466 V, 1.524 mA/cm 2, , 51.95%, and 0.37% respectively. ZnO nanorods were successfully synthesized by the plasma torch with the zinc powder as the source of ZnO.

The aim of this study is to determine the nanocrystalline size by using Williamson-Hall method of Fe80Cr20 powder which prepared by mechanical alloying process. X-rays diffraction line profile analysis was adopted to analyze the crystallite size and microstrains of Fe80Cr20 alloys powder. Transmission Electron Microscopy (TEM) was used to examine the microstructure morphology of the nanosized of Fe80Cr20 alloys. The crystallite size, microstrain, and lattice parameters were estimated by Williamson–Hall plot. The results showed that the mechanical alloying processes resulted the final product in nanocrystalline size range (below 12 nm) which confirmed by TEM observation and XRD line profile analysis.

Abstract. The oxidation behaviour of developed Fe 80 Cr 20 alloy and commercial ferritic steel at 1173 -1373 K in air is studied. Effects of crystallite size and titanium implantation on the oxidation behaviour of specimens were analyzed based on oxide morphologies and microstructures. Oxide scales characterisations of specimen after oxidized were identified by X-ray diffraction (XRD). The surface morphology of oxide scales were examined with scanning electronic microscope (SEM) and energy dispersive X-ray analysis (EDX). The rate constant of oxidation were determined using Wagner method. The results show that crystallite size and titanium implantation has remarkably enhanced the oxidation resistance. The oxidation kinetics indicate that the developed Fe 80 Cr 20 as the finer crystallite size both unimplanted and implanted specimens show better performance.

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