Composite panels of various ply orientations and 1 to 2 mm thickness were tested in tension with a center notch to determine the translaminar fracture toughness and in bending with no notch to determine the bulk flexural strength and modulus. Carbon/epoxy panels with a variety of notch lengths and widths were subjected to laboratory air conditions before testing. Carbon/bismaleimide panels with one basic notch configuration were tested in three pretest exposure conditions: laboratory air, a 400-h exposure in a controlled moisture chamber, and a 4000 h exposure in a natural tropical environment.
The tests were performed to investigate the following effects on fracture and mechanical properties and on micro and macrofailure mechanisms of the laminates.
(a) Effects of notch width and length and ply orientation on translaminar fracture toughness were studied in 0/90 and 0/±60 carbon/epoxy laminates, including effects of notches produced by ballistic penetration.
(b) Effects of extended exposure to moisture and sunlight on fracture and mechanical properties were studied in various 0/90 layups of carbon/bismaleimide laminates. A direct comparison of controlled chamber and natural tropical moisture effects was made for two materials.
(c) The load-deflection macrobehavior of notched panels was noted and analyzed. Linear-elastic and J-integral analyses were used to determine critical values of stress intensity factor, K, at the onset of self-similar translaminar fracture. A simple splitting model was used to describe the interlaminar failure that competed with and often prevented the translaminar fracture.
(d) Scanning electron microscope fractography was used to investigate and contrast the microfailure mechanisms of the laminates. The differences in micromechanisms between carbon/epoxy and carbon/bismaleimide were related to differences in the macrofracture behavior of the materials.
Analysis was performed of the test procedures for determination of fracture toughness and flexural strength and modulus. The method used for fracture toughness and associated K, J, and displacement expressions were proposed for more general use in measuring translaminar fracture toughness of composites. Use of the four-point bending test for flexural strength and modulus revealed an error that can occur in this type of test that is not fully addressed in ASTM Test Methods for Flexural Properties of Unreinforced and Reinforced Plastics and Electrical Insulating Materials (D 790-86).
A program was undertaken to apply the ASTM E 1221 test method to two submarine steels exhibiting high ratios of toughness to yield stress. The objective was to measure the capacities of these steels and representative shipyard welds to arrest fast running cracks. Although the method is not a measure of dynamic toughness, it was considered to be a procedure capable of comparing the crack arresting abilities of these steels.
The work has shown that it is possible to follow ASTM E 1221 and obtain valid crack arrest fracture toughness results for materials with room temperature KJc as high as 240 MPa√m and a yield stress of 690 MPa using specimens of 50-mm thickness. The process did, however, have a high level of unreliability, necessitating a large number of tests and extensive re-testing to obtain valid results. Test temperatures below −60°C were required to obtain run-arrest events, and as such could not easily be related to material qualification procedures such as explosion bulge testing or to submarine operating temperatures.
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