Die einstufige reduktive Reaktion mit Dimethylamin, Triethylphosphin oder Tri‐n‐propylphosphin wandelt Mo(III)‐chlorid und ‐bromid in die Mo(II)‐Dimeren (I) mit Mo‐Mo‐Bindung um.
Die Reaktion der monomeren trans‐ Komplexe (I) mit siedender Carbonsäure/Carbonsäureanhydrid führt zu den u‐Oxobis‐[u‐carboxylato]‐diosmium(IV)‐Komplexen (II).
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